1-(2-phenyl-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)-1H-benzo[d][1,2,3]triazole

Base Information

Chemical Name:1-(2-phenyl-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)-1H-benzo[d][1,2,3]triazole
CAS No.:1449418-23-8
Molecular Formula:C₂₃H₃₀N₄O
Molecular Weight:378.517
Hs Code.:

Synonyms:1-(2-phenyl-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)-1H-benzo[d][1,2,3]triazole

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Chemical Property of 1-(2-phenyl-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)-1H-benzo[d][1,2,3]triazole

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Technology Process of 1-(2-phenyl-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)-1H-benzo[d][1,2,3]triazole

There total 3 articles about 1-(2-phenyl-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)-1H-benzo[d][1,2,3]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1449418-01-2
1-(2-azido-1-phenylethoxy)-2,2,6,6-tetramethylpiperidine

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 1449418-23-8
1-(2-phenyl-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: With cesium fluoride; In acetonitrile; at 70 ℃; for 17h;
DOI:10.1021/ol402106x

Reference yield:

: 2564-83-2
2,2,6,6-tetramethyl-piperidine-N-oxyl

: 1449418-23-8
1-(2-phenyl-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium; naphthalene / tetrahydrofuran / 20 °C / Inert atmosphere

2: 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one / tetrahydrofuran; dichloromethane / 6 h / 20 °C / Inert atmosphere

3: cesium fluoride / acetonitrile / 17 h / 70 °C

With naphthalene; sodium; cesium fluoride; 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ol402106x

Reference yield:

: 211562-21-9
sodium 2,2,6,6-tetramethylpiperidine-1-oxide

: 1449418-23-8
1-(2-phenyl-2-((2,2,6,6-tetramethylpiperidin-1-yl)oxy)ethyl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one / tetrahydrofuran; dichloromethane / 6 h / 20 °C / Inert atmosphere

2: cesium fluoride / acetonitrile / 17 h / 70 °C

With cesium fluoride; 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ol402106x