1-(2-azido-1-phenylethoxy)-2,2,6,6-tetramethylpiperidine

Base Information

Chemical Name:1-(2-azido-1-phenylethoxy)-2,2,6,6-tetramethylpiperidine
CAS No.:1449418-01-2
Molecular Formula:C₁₇H₂₆N₄O
Molecular Weight:302.42
Hs Code.:

Synonyms:1-(2-azido-1-phenylethoxy)-2,2,6,6-tetramethylpiperidine

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Chemical Property of 1-(2-azido-1-phenylethoxy)-2,2,6,6-tetramethylpiperidine

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Technology Process of 1-(2-azido-1-phenylethoxy)-2,2,6,6-tetramethylpiperidine

There total 5 articles about 1-(2-azido-1-phenylethoxy)-2,2,6,6-tetramethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 211562-21-9
sodium 2,2,6,6-tetramethylpiperidine-1-oxide

: 1449418-01-2
1-(2-azido-1-phenylethoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:: With 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In tetrahydrofuran; dichloromethane; at 20 ℃; for 6h; Temperature; Time; Inert atmosphere;
DOI:10.1021/ol402106x

Reference yield: 92.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 1449418-01-2
1-(2-azido-1-phenylethoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:: With trimethylsilylazide; C₇H₁₅IO₄S; In dichloromethane; at 35 ℃; for 15h; Solvent; Reagent/catalyst; Wavelength; regioselective reaction; Sealed tube; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.9b03910

Reference yield: 92.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1449418-01-2
1-(2-azido-1-phenylethoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:: With sodium azide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trimethylsulfonium [bis(azido)iodate(I)]; In N,N-dimethyl-formamide; at 35 ℃; for 12h; Inert atmosphere; Irradiation;
DOI:10.1039/c9cc00007k