2-Methoxy-6-(6-methoxy-4-((1-phenyl-1H-1,2,3-triazol-4-yl)methoxy)benzofuran-2-yl)imidazo[2,1-b][1,3,4]thiadiazole

Base Information

Chemical Name:2-Methoxy-6-(6-methoxy-4-((1-phenyl-1H-1,2,3-triazol-4-yl)methoxy)benzofuran-2-yl)imidazo[2,1-b][1,3,4]thiadiazole
CAS No.:1476847-69-4
Molecular Formula:C₂₃H₁₈N₆O₄S
Molecular Weight:474.5
Hs Code.:

Synonyms:2-Methoxy-6-(6-methoxy-4-((1-phenyl-1H-1,2,3-triazol-4-yl)methoxy)benzofuran-2-yl)imidazo[2,1-b][1,3,4]thiadiazole

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Chemical Property of 2-Methoxy-6-(6-methoxy-4-((1-phenyl-1H-1,2,3-triazol-4-yl)methoxy)benzofuran-2-yl)imidazo[2,1-b][1,3,4]thiadiazole

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Technology Process of 2-Methoxy-6-(6-methoxy-4-((1-phenyl-1H-1,2,3-triazol-4-yl)methoxy)benzofuran-2-yl)imidazo[2,1-b][1,3,4]thiadiazole

There total 7 articles about 2-Methoxy-6-(6-methoxy-4-((1-phenyl-1H-1,2,3-triazol-4-yl)methoxy)benzofuran-2-yl)imidazo[2,1-b][1,3,4]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1476847-70-7
2-methoxy-6-(6-methoxy-4-(prop-2-yn-1-yloxy)benzofuran-2-yl)imidazo[2,1-b][1,3,4]thiadiazole

: 622-37-7
Phenyl azide

: 1476847-69-4
2-Methoxy-6-(6-methoxy-4-((1-phenyl-1H-1,2,3-triazol-4-yl)methoxy)benzofuran-2-yl)imidazo[2,1-b][1,3,4]thiadiazole

Guidance literature:: In N,N-dimethyl-formamide;

Reference yield:

: 1476847-55-8
6-(4-(benzyloxy)-6-methoxybenzofuran-2-yl)-2-methoxyimidazo[2,1-b][1,3,4]thiadiazole

: 1476847-69-4
2-Methoxy-6-(6-methoxy-4-((1-phenyl-1H-1,2,3-triazol-4-yl)methoxy)benzofuran-2-yl)imidazo[2,1-b][1,3,4]thiadiazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: pentamethylbenzene,; boron trichloride / dichloromethane / 1.05 h / -78 °C / Inert atmosphere

2.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / tetrahydrofuran / 0.42 h / Inert atmosphere

2.2: 1 h / 20 °C / Sonication; Inert atmosphere

3.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; tributylphosphine; pentamethylbenzene,; boron trichloride; sodium L-ascorbate; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1476847-56-9
6-methoxy-2-(2-methoxyimidazolo[2,1-b][1,3,4]thiadiazol-6-yl)benzofuran-4-ol

: 1476847-69-4
2-Methoxy-6-(6-methoxy-4-((1-phenyl-1H-1,2,3-triazol-4-yl)methoxy)benzofuran-2-yl)imidazo[2,1-b][1,3,4]thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / tetrahydrofuran / 0.42 h / Inert atmosphere

1.2: 1 h / 20 °C / Sonication; Inert atmosphere

2.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; tributylphosphine; sodium L-ascorbate; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; N,N-dimethyl-formamide;