2-(2,4-Dinitro-phenyl)-N-(4-iodo-phenyl)-2-[(4-nitro-phenyl)-hydrazono]-thioacetamide

Base Information

Chemical Name:2-(2,4-Dinitro-phenyl)-N-(4-iodo-phenyl)-2-[(4-nitro-phenyl)-hydrazono]-thioacetamide
CAS No.:79865-73-9
Molecular Formula:C₂₀H₁₃IN₆O₆S
Molecular Weight:592.33
Hs Code.:

Synonyms:2-(2,4-Dinitro-phenyl)-N-(4-iodo-phenyl)-2-[(4-nitro-phenyl)-hydrazono]-thioacetamide

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Chemical Property of 2-(2,4-Dinitro-phenyl)-N-(4-iodo-phenyl)-2-[(4-nitro-phenyl)-hydrazono]-thioacetamide

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Technology Process of 2-(2,4-Dinitro-phenyl)-N-(4-iodo-phenyl)-2-[(4-nitro-phenyl)-hydrazono]-thioacetamide

There total 3 articles about 2-(2,4-Dinitro-phenyl)-N-(4-iodo-phenyl)-2-[(4-nitro-phenyl)-hydrazono]-thioacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 100-05-0
4-nitrobenzenediazonium chloride

: 79865-62-6
2-(2,4-Dinitro-phenyl)-N-(4-iodo-phenyl)-3-oxo-thiobutyramide

: 79865-73-9
2-(2,4-Dinitro-phenyl)-N-(4-iodo-phenyl)-2-[(4-nitro-phenyl)-hydrazono]-thioacetamide

Guidance literature:: In ethanol; at 0 ℃;

Reference yield:

: 2200-86-4
1-(2,4-dinitrophenyl)propan-2-one

: 79865-73-9
2-(2,4-Dinitro-phenyl)-N-(4-iodo-phenyl)-2-[(4-nitro-phenyl)-hydrazono]-thioacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium tert-butoxide / 1.) acetonitrile; 2.) room temperature, 24 h

2: 86 percent / aq. ethanol / 0 °C

With sodium t-butanolate; In ethanol;

Reference yield:

: 2059-76-9
4-iodophenyl isothiocyanate

: 79865-73-9
2-(2,4-Dinitro-phenyl)-N-(4-iodo-phenyl)-2-[(4-nitro-phenyl)-hydrazono]-thioacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium tert-butoxide / 1.) acetonitrile; 2.) room temperature, 24 h

2: 86 percent / aq. ethanol / 0 °C

With sodium t-butanolate; In ethanol;