(Zn((NC₄H₂CC₆H₃(C(CH₃)3)2)2(NC₄H₂C₂)(NC₄H₂CH)))2

Base Information

Chemical Name:(Zn((NC₄H₂CC₆H₃(C(CH₃)3)2)2(NC₄H₂C₂)(NC₄H₂CH)))2
CAS No.:278807-35-5
Molecular Formula:C₉₈H₁₀₂N₈Zn₂
Molecular Weight:1522.72
Hs Code.:

(Zn((NC<sub>4</sub>H<sub>2</sub>CC<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)2(NC<sub>4</sub>H<sub>2</sub>C<sub>2</sub>)(NC<sub>4</sub>H<sub>2</sub>CH)))2

Synonyms:(Zn((NC₄H₂CC₆H₃(C(CH₃)3)2)2(NC₄H₂C₂)(NC₄H₂CH)))2

Suppliers and Price of (Zn((NC₄H₂CC₆H₃(C(CH₃)3)2)2(NC₄H₂C₂)(NC₄H₂CH)))2

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Chemical Property of (Zn((NC₄H₂CC₆H₃(C(CH₃)3)2)2(NC₄H₂C₂)(NC₄H₂CH)))2

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Technology Process of (Zn((NC₄H₂CC₆H₃(C(CH₃)3)2)2(NC₄H₂C₂)(NC₄H₂CH)))2

There total 3 articles about (Zn((NC₄H₂CC₆H₃(C(CH₃)3)2)2(NC₄H₂C₂)(NC₄H₂CH)))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 294183-82-7
[5-ethynyl-10,20-bis[3',5'-(di-tert-butyl)phenyl]porphinato]zinc(II)

: 294183-84-9
[5,15-bis(3',5'-di-tert-butylphenyl)-10-bromoporphyrinato]zinc(II)

: 278807-35-5
[(NCCHCHCC(C₆H₃(C(CH₃)3)2))2(NCCHCHCC(C))(NCCHCHCCH)Zn]2

Guidance literature:: With Pd₂(dibenzylideneacetone)3/PPh₃; CuI; Et₃N/C₅H₅N; In pyridine; triethylamine; toluene; Ethynylporphyrin, bromoporphyrin, Pd compd., PPh3, CuI were dried (vac.)and dissolved in toluene, pyridine and Et3N; soln. was degassed and sti rred at 80°C for 1.5 h under inert atm; passed through silica plug; chromd. (SiO2, petroleum ether/CH2Cl2/pyridine; pyridine/CHCl3); crystd. (CHCl3/methanol);
DOI:10.1039/b109915a

Reference yield: 61.0%

: 294183-82-7
[5-ethynyl-10,20-bis[3',5'-(di-tert-butyl)phenyl]porphinato]zinc(II)

: C₂₇H₃₄BF₂IN₂

: 278807-35-5
(Zn((NC₄H₂CC₆H₃(C(CH₃)3)2)2(NC₄H₂C₂)(NC₄H₂CH)))2

: C₇₇H₈₅BF₂N₆Zn

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In toluene; at 50 ℃; for 15h; Inert atmosphere;
DOI:10.1039/c7cc07049g

Reference yield: 18.0%

: 220355-76-0
[5,15-bis[3,5-di(tert-butyl)phenyl]-10-iodoporphyrinato(2-)-κN(21),κN(22),κN(23),κN(24)]zinc(II)

: 1066-54-2
trimethylsilylacetylene

: 817563-40-9
(Zn((NC₄H₂CC₆H₃(C(CH₃)3)2)2(NC₄H₂C₃)(NC₄H₂CH)))2

: 278807-35-5
(Zn((NC₄H₂CC₆H₃(C(CH₃)3)2)2(NC₄H₂C₂)(NC₄H₂CH)))2

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In water; benzene; at 60 ℃; for 48h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.201700891