5-Benzyl-3,6-dihydro-1-(2-isopropenylphenyl)-6-oxo-3-phenyl-1-pyrimidinium-4-olat

Base Information

• Chemical Name: 5-Benzyl-3,6-dihydro-1-(2-isopropenylphenyl)-6-oxo-3-phenyl-1-pyrimidinium-4-olat
• CAS No.: 112794-56-6
• Molecular Formula: C₂₆H₂₂N₂O₂
• Molecular Weight: 394.473

Synonyms:5-Benzyl-3,6-dihydro-1-(2-isopropenylphenyl)-6-oxo-3-phenyl-1-pyrimidinium-4-olat

Chemical Property of 5-Benzyl-3,6-dihydro-1-(2-isopropenylphenyl)-6-oxo-3-phenyl-1-pyrimidinium-4-olat

Chemical Property:

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Technology Process of 5-Benzyl-3,6-dihydro-1-(2-isopropenylphenyl)-6-oxo-3-phenyl-1-pyrimidinium-4-olat

There total 1 articles about 5-Benzyl-3,6-dihydro-1-(2-isopropenylphenyl)-6-oxo-3-phenyl-1-pyrimidinium-4-olat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(2,4,6-trichlorophenyl)-2-benzylmalonate (15781-74-5) + 2-isopropenylaniline (52562-19-3) + ethyl N-phenylformimidate (6780-49-0) → 5-Benzyl-3,6-dihydro-6-oxo-1,3-diphenyl-1-pyrimidinium-4-olat (101530-90-9) + 5-Benzyl-3,6-dihydro-1-(2-isopropenylphenyl)-6-oxo-3-phenyl-1-pyrimidinium-4-olat (112794-56-6)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given; 1) 20 h, 20 deg C, 2) 10 min, 150 deg C;

Reference yield: 84.0%

5-Benzyl-3,6-dihydro-1-(2-isopropenylphenyl)-6-oxo-3-phenyl-1-pyrimidinium-4-olat (112794-56-6) → 6-Benzyl-4-methyl-8-phenylbenzo-1,8-diazatricyclo<4.3.1.04,9>dec-2-en-7,10-dion (112794-58-8)

Guidance literature:

In xylene; at 190 ℃; for 30h;

upstream raw materials:

bis(2,4,6-trichlorophenyl)-2-benzylmalonate

2-isopropenylaniline

ethyl N-phenylformimidate

Downstream raw materials:

6-Benzyl-4-methyl-8-phenylbenzo-1,8-diazatricyclo<4.3.1.0^4,9>dec-2-en-7,10-dion

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