(E)-1-(iodophenylmethylene)-2,3,4-trihydro-1H-benzo[d]pyrido[1,2-a]imidazole

Base Information

Chemical Name:(E)-1-(iodophenylmethylene)-2,3,4-trihydro-1H-benzo[d]pyrido[1,2-a]imidazole
CAS No.:1314451-62-1
Molecular Formula:C₁₈H₁₅IN₂
Molecular Weight:386.235
Hs Code.:

Synonyms:(E)-1-(iodophenylmethylene)-2,3,4-trihydro-1H-benzo[d]pyrido[1,2-a]imidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(iodophenylmethylene)-2,3,4-trihydro-1H-benzo[d]pyrido[1,2-a]imidazole

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Technology Process of (E)-1-(iodophenylmethylene)-2,3,4-trihydro-1H-benzo[d]pyrido[1,2-a]imidazole

There total 6 articles about (E)-1-(iodophenylmethylene)-2,3,4-trihydro-1H-benzo[d]pyrido[1,2-a]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1276539-66-2
2-(5-phenylpent-4-ynyl)-1H-benzo[d]imidazole

: 1314451-62-1
(E)-1-(iodophenylmethylene)-2,3,4-trihydro-1H-benzo[d]pyrido[1,2-a]imidazole

Guidance literature:: With iodine; sodium carbonate; silver nitrate; In tetrahydrofuran; at 20 ℃; for 60h;
DOI:10.1002/adsc.201100038

Reference yield:

: C₁₈H₁₈N₂O

: 1314451-62-1
(E)-1-(iodophenylmethylene)-2,3,4-trihydro-1H-benzo[d]pyrido[1,2-a]imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 5 h / 90 °C / Inert atmosphere

2: iodine; sodium carbonate; silver nitrate / tetrahydrofuran / 60 h / 20 °C

With iodine; sodium carbonate; silver nitrate; acetic acid; In tetrahydrofuran;
DOI:10.1002/adsc.201100038

Reference yield:

: 77758-51-1
methyl hex-5-ynoate

: 1314451-62-1
(E)-1-(iodophenylmethylene)-2,3,4-trihydro-1H-benzo[d]pyrido[1,2-a]imidazole

Guidance literature:: Multi-step reaction with 5 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diethylamine / 2 h / 20 °C

2: potassium hydroxide / tetrahydrofuran; water / 3 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / methanol / 20 °C

4: acetic acid / 5 h / 90 °C / Inert atmosphere

5: iodine; sodium carbonate; silver nitrate / tetrahydrofuran / 60 h / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; iodine; sodium carbonate; silver nitrate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; potassium hydroxide; In tetrahydrofuran; methanol; water; 1: Sonogashira coupling;
DOI:10.1002/adsc.201100038