Benzyl-[(1S,2R,3S)-3-(tert-butyl-dimethyl-silanyloxy)-1-((E)-styryl)-2-triethylsilanyloxymethyl-butyl]-amine

Base Information

Chemical Name:Benzyl-[(1S,2R,3S)-3-(tert-butyl-dimethyl-silanyloxy)-1-((E)-styryl)-2-triethylsilanyloxymethyl-butyl]-amine
CAS No.:142065-10-9
Molecular Formula:C₃₂H₅₃NO₂Si₂
Molecular Weight:539.949
Hs Code.:

Synonyms:Benzyl-[(1S,2R,3S)-3-(tert-butyl-dimethyl-silanyloxy)-1-((E)-styryl)-2-triethylsilanyloxymethyl-butyl]-amine

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Chemical Property of Benzyl-[(1S,2R,3S)-3-(tert-butyl-dimethyl-silanyloxy)-1-((E)-styryl)-2-triethylsilanyloxymethyl-butyl]-amine

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Technology Process of Benzyl-[(1S,2R,3S)-3-(tert-butyl-dimethyl-silanyloxy)-1-((E)-styryl)-2-triethylsilanyloxymethyl-butyl]-amine

There total 9 articles about Benzyl-[(1S,2R,3S)-3-(tert-butyl-dimethyl-silanyloxy)-1-((E)-styryl)-2-triethylsilanyloxymethyl-butyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 994-30-9
triethylsilyl chloride

: 142039-68-7
(E)-(2R,3S)-3-Benzylamino-2-[(S)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-5-phenyl-pent-4-en-1-ol

: 142065-10-9
Benzyl-[(1S,2R,3S)-3-(tert-butyl-dimethyl-silanyloxy)-1-((E)-styryl)-2-triethylsilanyloxymethyl-butyl]-amine

Guidance literature:: With 1H-imidazole; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1246/bcsj.68.2103

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 142065-10-9
Benzyl-[(1S,2R,3S)-3-(tert-butyl-dimethyl-silanyloxy)-1-((E)-styryl)-2-triethylsilanyloxymethyl-butyl]-amine

Guidance literature:: Multi-step reaction with 3 steps

2: 60 percent / LAH

With lithium aluminium tetrahydride;
DOI:10.1021/ja00039a066

Reference yield:

: 142039-50-7
C₂₁H₂₅NO₃S

: 142065-10-9
Benzyl-[(1S,2R,3S)-3-(tert-butyl-dimethyl-silanyloxy)-1-((E)-styryl)-2-triethylsilanyloxymethyl-butyl]-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) -78 deg C

3: 60 percent / LAH

With lithium aluminium tetrahydride;
DOI:10.1021/ja00039a066