N-<(4-Methoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>-2,6-difluorbenzolsulfonsaeureamid

Base Information

Chemical Name:N-<(4-Methoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>-2,6-difluorbenzolsulfonsaeureamid
CAS No.:121583-55-9
Molecular Formula:C₁₃H₁₁Cl₃F₂N₄O₃S
Molecular Weight:447.677
Hs Code.:

Synonyms:N-<(4-Methoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>-2,6-difluorbenzolsulfonsaeureamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(4-Methoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>-2,6-difluorbenzolsulfonsaeureamid

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Technology Process of N-<(4-Methoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>-2,6-difluorbenzolsulfonsaeureamid

There total 2 articles about N-<(4-Methoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>-2,6-difluorbenzolsulfonsaeureamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60230-37-7
2,6-difluorobenzene-1-sulfonamide

: 121583-55-9
N-<(4-Methoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>-2,6-difluorbenzolsulfonsaeureamid

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / conc. HCl / 16 h / Heating

2: SOCl₂ / 2 h / Heating

3: Et₃N / toluene / 18 h / Ambient temperature

With hydrogenchloride; thionyl chloride; triethylamine; In toluene;
DOI:10.1007/BF00810285

Reference yield:

: 121583-28-6
N-(2,2,2-Trichlor-1-hydroxyethyl)-2,6-difluorbenzolsaeureamid

: 121583-55-9
N-<(4-Methoxypyrimidin-2-ylamino)-2,2,2-trichlorethyl>-2,6-difluorbenzolsulfonsaeureamid

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 2 h / Heating

2: Et₃N / toluene / 18 h / Ambient temperature

With thionyl chloride; triethylamine; In toluene;
DOI:10.1007/BF00810285