Phenylhydrazone of 2-acetoxyamino-2-methyl-1-phenyl-1-propanone

Base Information

• Chemical Name: Phenylhydrazone of 2-acetoxyamino-2-methyl-1-phenyl-1-propanone
• CAS No.: 107259-88-1
• Molecular Formula: C₁₈H₂₁N₃O₂
• Molecular Weight: 311.384
• Mol file: 107259-88-1.mol

Synonyms:Phenylhydrazone of 2-acetoxyamino-2-methyl-1-phenyl-1-propanone

Chemical Property of Phenylhydrazone of 2-acetoxyamino-2-methyl-1-phenyl-1-propanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phenylhydrazone of 2-acetoxyamino-2-methyl-1-phenyl-1-propanone

There total 3 articles about Phenylhydrazone of 2-acetoxyamino-2-methyl-1-phenyl-1-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

acetic anhydride (108-24-7) + Phenylhydrazone of 2-Hydroxyamino-2-methyl-1-phenyl-1-propanone (107259-84-7) → Phenylhydrazone of 2-acetoxyamino-2-methyl-1-phenyl-1-propanone (107259-88-1)

Guidance literature:

In diethyl ether;

DOI:10.1007/BF00514996

Reference yield:

phenylhydrazine (100-63-0) → Phenylhydrazone of 2-acetoxyamino-2-methyl-1-phenyl-1-propanone (107259-88-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / 50percent aqueous acetic acid / ethanol / 2 h

2: 70 percent / diethyl ether

With acetic acid; In diethyl ether; ethanol;

DOI:10.1007/BF00514996

Reference yield:

2-(hydroxyamino)-2-methyl-1-phenylpropan-1-one (34046-70-3) → Phenylhydrazone of 2-acetoxyamino-2-methyl-1-phenyl-1-propanone (107259-88-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / 50percent aqueous acetic acid / ethanol / 2 h

2: 70 percent / diethyl ether

With acetic acid; In diethyl ether; ethanol;

DOI:10.1007/BF00514996

upstream raw materials:

acetic anhydride

Phenylhydrazone of 2-Hydroxyamino-2-methyl-1-phenyl-1-propanone

phenylhydrazine

2-(hydroxyamino)-2-methyl-1-phenylpropan-1-one

Downstream raw materials:

4,5-dihydro-5,5-dimethyl-1,3-diphenyl-1H-1,2,4-triazole