1-(2,2'-dimethoxytriphenylmethoxy)-2-[(9-fluorenylmethoxy-carbonyl)amino]-propan-3-ol

Base Information

• Chemical Name: 1-(2,2'-dimethoxytriphenylmethoxy)-2-[(9-fluorenylmethoxy-carbonyl)amino]-propan-3-ol
• CAS No.: 154928-39-9
• Molecular Formula: C₃₉H₃₇NO₆
• Molecular Weight: 615.726

Synonyms:1-(2,2'-dimethoxytriphenylmethoxy)-2-[(9-fluorenylmethoxy-carbonyl)amino]-propan-3-ol

Chemical Property of 1-(2,2'-dimethoxytriphenylmethoxy)-2-[(9-fluorenylmethoxy-carbonyl)amino]-propan-3-ol

Chemical Property:

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Technology Process of 1-(2,2'-dimethoxytriphenylmethoxy)-2-[(9-fluorenylmethoxy-carbonyl)amino]-propan-3-ol

There total 2 articles about 1-(2,2'-dimethoxytriphenylmethoxy)-2-[(9-fluorenylmethoxy-carbonyl)amino]-propan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide (82911-69-1) → 1-(2,2'-dimethoxytriphenylmethoxy)-2-[(9-fluorenylmethoxy-carbonyl)amino]-propan-3-ol (154928-39-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / dimethylformamide / 24 h

2: 59 percent / 4-(dimethylamino)pyridine; pyridine / 2 h

With pyridine; dmap; In N,N-dimethyl-formamide;

DOI:10.1016/S0960-894X(00)00673-9

Reference yield:

→ 1-(2,2'-dimethoxytriphenylmethoxy)-2-[(9-fluorenylmethoxy-carbonyl)amino]-propan-3-ol (154928-39-9)

Guidance literature:

Reference yield: 98.0%

1-(2,2'-dimethoxytriphenylmethoxy)-2-[(9-fluorenylmethoxy-carbonyl)amino]-propan-3-ol (154928-39-9) → 2-amino-1-O-(4,4'-dimethoxytrityl)propane-1,3-diol (154928-41-3)

Guidance literature:

With piperidine; In N,N-dimethyl-formamide; for 3h;

DOI:10.1016/S0960-894X(00)00673-9

upstream raw materials:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

Downstream raw materials:

2-amino-1-O-(4,4'-dimethoxytrityl)propane-1,3-diol

[2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-{[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethyl]-amide} 4'-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

succinic acid mono-[3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-({4'-[2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethylcarbamoyl]-[2,2']bipyridinyl-4-carbonyl}-amino)-propyl] ester

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