[2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Base Information

Chemical Name:[2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)
CAS No.:331465-53-3
Molecular Formula:C₆₀H₅₈N₄O₁₀
Molecular Weight:995.141
Hs Code.:

Synonyms:[2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Suppliers and Price of [2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

There total 3 articles about [2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 154928-41-3
2-amino-1-O-(4,4'-dimethoxytrityl)propane-1,3-diol

: 331465-52-2
2,2'-bipyridine-4,4'-dicarboxylic acid pentafluorophenolic ester

: 331465-53-3
[2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/S0960-894X(00)00673-9

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 331465-53-3
[2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / 4-(dimethylamino)pyridine; pyridine / 2 h

2: 98 percent / piperidine / dimethylformamide / 3 h

3: 85 percent / pyridine / dimethylformamide / 20 °C

With piperidine; pyridine; dmap; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(00)00673-9

Reference yield:

: 154928-39-9
1-(2,2'-dimethoxytriphenylmethoxy)-2-[(9-fluorenylmethoxy-carbonyl)amino]-propan-3-ol

: 331465-53-3
[2,2']bipyridinyl-4,4'-dicarboxylic acid bis-({2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-amide)

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / piperidine / dimethylformamide / 3 h

2: 85 percent / pyridine / dimethylformamide / 20 °C

With piperidine; pyridine; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(00)00673-9