triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate

Base Information

Chemical Name:triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate
CAS No.:1307908-04-8
Molecular Formula:C₆₉H₉₀N₂O₁₁Si
Molecular Weight:1151.57
Hs Code.:

Synonyms:triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate

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Chemical Property of triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate

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Technology Process of triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate

There total 11 articles about triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1307908-00-4
4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoic acid

: 1307907-79-4
triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate

: 1307908-04-8
triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c0jm04570e

Reference yield:

: 106817-36-1
4-(4-dodecyloxybenzoyloxy)benzoyl chloride

: 1307908-04-8
triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 12 h / 20 °C

2: dicyclohexyl-carbodiimide / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere

With triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/c0jm04570e

Reference yield:

: 1307907-96-5
methyl 4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoate

: 1307908-04-8
triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol; water

2: dicyclohexyl-carbodiimide / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere

With dicyclohexyl-carbodiimide; potassium hydroxide; In ethanol; dichloromethane; water;
DOI:10.1039/c0jm04570e