triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate

Base Information

Chemical Name:triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate
CAS No.:1307907-79-4
Molecular Formula:C₄₂H₅₈O₈Si
Molecular Weight:719.003
Hs Code.:

Synonyms:triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate

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Chemical Property of triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate

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Technology Process of triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate

There total 4 articles about triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 703404-59-5
3,5-dihydroxy-triisopropylsilyl benzoate

: 106817-36-1
4-(4-dodecyloxybenzoyloxy)benzoyl chloride

: 1307907-79-4
triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1039/c0jm04570e

Reference yield:

: 2312-15-4
p-dodecyloxybenzoic acid

: 1307907-79-4
triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: 20 % Pd(OH)2/C; hydrogen / tetrahydrofuran / 7 h / 45004.5 Torr

3: oxalyl dichloride / dichloromethane / 4 h / 20 °C

4: triethylamine / dichloromethane / 12 h / 20 °C

With dmap; oxalyl dichloride; 20 % Pd(OH)2/C; hydrogen; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c0jm04570e

Reference yield:

: 94-18-8
Benzyl 4-hydroxybenzoate

: 1307907-79-4
triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: 20 % Pd(OH)2/C; hydrogen / tetrahydrofuran / 7 h / 45004.5 Torr

3: oxalyl dichloride / dichloromethane / 4 h / 20 °C

4: triethylamine / dichloromethane / 12 h / 20 °C

With dmap; oxalyl dichloride; 20 % Pd(OH)2/C; hydrogen; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c0jm04570e