3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoic acid

Base Information

Chemical Name:3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoic acid
CAS No.:1307907-54-5
Molecular Formula:C₆₀H₇₀N₂O₁₁
Molecular Weight:995.223
Hs Code.:

Synonyms:3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoic acid

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Chemical Property of 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoic acid

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Technology Process of 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoic acid

There total 13 articles about 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1307908-04-8
triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate

: 1307907-54-5
3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoic acid

Guidance literature:: triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoate; With tetrabutyl ammonium fluoride; In dichloromethane; at -78 ℃; for 2h; Inert atmosphere;

With acetic acid; In dichloromethane;
DOI:10.1039/c0jm04570e

Reference yield:

: 1307907-79-4
triisopropylsilyl 3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-hydroxybenzoate

: 1307907-54-5
3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / dichloromethane / 2 h / -78 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/c0jm04570e

Reference yield:

: 106817-36-1
4-(4-dodecyloxybenzoyloxy)benzoyl chloride

: 1307907-54-5
3-{4-[4-(dodecyloxy)benzoyloxy]benzoyloxy}-5-(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyloxy)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 12 h / 20 °C

2: dicyclohexyl-carbodiimide / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / dichloromethane / 2 h / -78 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/c0jm04570e