1-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-5-methyl-1H-pyrimidine-2,4-dione

Base Information

Chemical Name:1-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-5-methyl-1H-pyrimidine-2,4-dione
CAS No.:200931-81-3
Molecular Formula:C₃₄H₃₄N₂O₇
Molecular Weight:582.653
Hs Code.:

1-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-5-methyl-1H-pyrimidine-2,4-dione

Synonyms:1-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-5-methyl-1H-pyrimidine-2,4-dione

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Chemical Property of 1-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-5-methyl-1H-pyrimidine-2,4-dione

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Technology Process of 1-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-5-methyl-1H-pyrimidine-2,4-dione

There total 3 articles about 1-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-5-methyl-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 239808-67-4
4,4’-dimethoxytrityl trifluoromethanesulfonate

: 200931-79-9
(5'R,6'R)-1-(2'-deoxy-3',5'-ethano-5',6'-methano-β-D-ribofuranosyl)thymine

: 200931-81-3
1-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-5-methyl-1H-pyrimidine-2,4-dione

Guidance literature:: With pyridine; for 6h; Ambient temperature;
DOI:10.1002/hlca.19970800812

Reference yield:

: 1-[(1aR,1bS,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-5-methyl-1H-pyrimidine-2,4-dione

: 200931-81-3
1-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-5-methyl-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: Bn₄NF / tetrahydrofuran; hexane / 0.02 h / Ambient temperature

2: 93 percent / Bn₄NF / tetrahydrofuran; hexane / 3 h / Ambient temperature

3: 70 percent / pyridine / 6 h / Ambient temperature

With pyridine; Bn₄NF; In tetrahydrofuran; hexane;
DOI:10.1002/hlca.19970800812

Reference yield:

: 200931-77-7
1-[(1aR,1bS,3R,4aS,5aR)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-5-methyl-1H-pyrimidine-2,4-dione

: 200931-81-3
1-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-5-methyl-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Bn₄NF / tetrahydrofuran; hexane / 3 h / Ambient temperature

2: 70 percent / pyridine / 6 h / Ambient temperature

With pyridine; Bn₄NF; In tetrahydrofuran; hexane;
DOI:10.1002/hlca.19970800812