S-[(trans-4-aminocyclohexyl)methyl]ethanethioate trifluoroacetate

Base Information

Chemical Name:S-[(trans-4-aminocyclohexyl)methyl]ethanethioate trifluoroacetate
CAS No.:1607590-28-2
Molecular Formula:C₂HF₃O₂*C₉H₁₇NOS
Molecular Weight:301.33
Hs Code.:

Synonyms:S-[(trans-4-aminocyclohexyl)methyl]ethanethioate trifluoroacetate

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Chemical Property of S-[(trans-4-aminocyclohexyl)methyl]ethanethioate trifluoroacetate

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Technology Process of S-[(trans-4-aminocyclohexyl)methyl]ethanethioate trifluoroacetate

There total 3 articles about S-[(trans-4-aminocyclohexyl)methyl]ethanethioate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1418200-25-5
trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester

: 76-05-1
trifluoroacetic acid

: 1607590-28-2
S-[(trans-4-aminocyclohexyl)methyl]ethanethioate trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 239074-29-4
trans (4-hydroxymethyl-cyclohexyl)-carbamic acid tert-butyl ester

: 1607590-28-2
S-[(trans-4-aminocyclohexyl)methyl]ethanethioate trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine / dichloromethane; water / 20 °C

2: dimethyl sulfoxide / 3 h / 55 °C

3: dichloromethane / 2 h / 20 °C

With dmap; triethylamine; In dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 947141-76-6
((1r,4r)-4-(tert-butoxycarbonylamino)cyclohexyl)methyl 4-methylbenzene-sulfonate

: 1607590-28-2
S-[(trans-4-aminocyclohexyl)methyl]ethanethioate trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide / 3 h / 55 °C

2: dichloromethane / 2 h / 20 °C

In dichloromethane; dimethyl sulfoxide;