2-methoxy-3-{N'-[5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester

Base Information

Chemical Name:2-methoxy-3-{N'-[5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester
CAS No.:787629-32-7
Molecular Formula:C₅₈H₇₈N₆O₁₃
Molecular Weight:1067.29
Hs Code.:

2-methoxy-3-{<i>N</i>'-[5-(<i>N</i>'-{2-methoxy-3-[<i>N</i>'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester

Synonyms:2-methoxy-3-{N'-[5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester

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Chemical Property of 2-methoxy-3-{N'-[5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester

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Technology Process of 2-methoxy-3-{N'-[5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester

There total 7 articles about 2-methoxy-3-{N'-[5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 288099-33-2
2-methoxyisophthalic acid monomethyl ester

: 787629-28-1
5-(N'-{2-Methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoic acid hydrazide

: 787629-32-7
2-methoxy-3-{N'-[5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/ja047436p

Reference yield:

: 255062-86-3
2-octyloxybenzoic acid hydrazide

: 787629-32-7
2-methoxy-3-{N'-[5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / DCC / CH₂Cl₂ / 3 h / 20 °C

2: 94 percent / hydrazine hydrate / methanol / 2 h / 40 °C

3: 83 percent / EDCI / CH₂Cl₂ / 3 h / 20 °C

4: 70 percent / hydrazine hydrate / methanol; tetrahydrofuran / 4 h / 40 °C

5: 33 percent / EDCI / CH₂Cl₂ / 3 h / 20 °C

With hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja047436p

Reference yield:

: 255062-85-2
2-octyloxybenzoic acid methyl ester

: 787629-32-7
2-methoxy-3-{N'-[5-(N'-{2-methoxy-3-[N'-(2-octyloxy-benzoyl)-hydrazinocarbonyl]-benzoyl}-hydrazinocarbonyl)-2,4-bis-octyloxy-benzoyl]-hydrazinocarbonyl}-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / hydrazine hydrate / methanol / 5 h / 40 °C

2: 88 percent / DCC / CH₂Cl₂ / 3 h / 20 °C

3: 94 percent / hydrazine hydrate / methanol / 2 h / 40 °C

4: 83 percent / EDCI / CH₂Cl₂ / 3 h / 20 °C

5: 70 percent / hydrazine hydrate / methanol; tetrahydrofuran / 4 h / 40 °C

6: 33 percent / EDCI / CH₂Cl₂ / 3 h / 20 °C

With hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja047436p