3-bromo-4-nitro-N-<<2-(trimethylsilyl)ethyl>sulfonyl>aniline

Base Information

• Chemical Name: 3-bromo-4-nitro-N-<<2-(trimethylsilyl)ethyl>sulfonyl>aniline
• CAS No.: 158531-07-8
• Molecular Formula: C₁₁H₁₇BrN₂O₄SSi
• Molecular Weight: 381.322
• Mol file: 158531-07-8.mol

Synonyms:3-bromo-4-nitro-N-<<2-(trimethylsilyl)ethyl>sulfonyl>aniline

Chemical Property of 3-bromo-4-nitro-N-<<2-(trimethylsilyl)ethyl>sulfonyl>aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 3-bromo-4-nitro-N-<<2-(trimethylsilyl)ethyl>sulfonyl>aniline

There total 1 articles about 3-bromo-4-nitro-N-<<2-(trimethylsilyl)ethyl>sulfonyl>aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-4-nitroaniline (40787-96-0) + 2-trimethylsilanyl-ethanesulfonyl chloride (106018-85-3) → 3-bromo-4-nitro-N-<<2-(trimethylsilyl)ethyl>sulfonyl>aniline (158531-07-8)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 1 h, 2.) DMF, 2 h;

DOI:10.1021/jm00046a028

Reference yield: 43.0%

potassium phtalimide (1074-82-4) + 3-bromo-4-nitro-N-<<2-(trimethylsilyl)ethyl>sulfonyl>aniline (158531-07-8) → N-<2-nitro-5-<<(trimethylsilyl)sulfonyl>amino>phenyl>phthalimide (158531-06-7)

Guidance literature:

With copper(l) iodide; In various solvent(s); for 4h; Heating;

DOI:10.1021/jm00046a028

upstream raw materials:

3-bromo-4-nitroaniline

2-trimethylsilanyl-ethanesulfonyl chloride

Downstream raw materials:

N-<2-nitro-5-<<(trimethylsilyl)sulfonyl>amino>phenyl>phthalimide