benzamidomethyl benzyl sulphide

Base Information

• Chemical Name: benzamidomethyl benzyl sulphide
• CAS No.: 51643-77-7
• Molecular Formula: C₁₅H₁₅NOS
• Molecular Weight: 257.356
• Mol file: 51643-77-7.mol

Synonyms:benzamidomethyl benzyl sulphide

Chemical Property of benzamidomethyl benzyl sulphide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of benzamidomethyl benzyl sulphide

There total 6 articles about benzamidomethyl benzyl sulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.6%

(benzoylaminomethyl)triethylammonium chloride (78134-74-4) + phenylmethanethiol (100-53-8) → benzamidomethyl benzyl sulphide (51643-77-7)

Guidance literature:

With triethylamine; In water; at 20 ℃; for 1h;

DOI:10.3390/50700927

Reference yield: 80.0%

benzoylaminothioacetic acid S-benzyl ester → benzamidomethyl benzyl sulphide (51643-77-7)

Guidance literature:

With manganese; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); 1,3-bis-(diphenylphosphino)propane; In toluene; at 150 ℃; for 12h; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.joc.1c01480

Reference yield:

N-(piperidinomethyl)benzamide (4380-83-0) + phenylmethanethiol (100-53-8) → benzamidomethyl benzyl sulphide (51643-77-7)

Guidance literature:

With sodium hydroxide; In toluene; Heating;

DOI:10.1248/cpb.21.2257

upstream raw materials:

N-<(diethylamino)methyl>benzamide

phenylmethanethiol

N-(chloromethyl)benzamide

N-(piperidinomethyl)benzamide