C₄₄H₂₇N₇

Base Information

Chemical Name:C₄₄H₂₇N₇
CAS No.:1537905-21-7
Molecular Formula:C₄₄H₂₇N₇
Molecular Weight:653.745
Hs Code.:

C<sub>44</sub>H<sub>27</sub>N<sub>7</sub>

Synonyms:C₄₄H₂₇N₇

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Chemical Property of C₄₄H₂₇N₇

Chemical Property:

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Technology Process of C₄₄H₂₇N₇

There total 8 articles about C₄₄H₂₇N₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1537905-34-2
2-iodo-5-phenyl-5H-benzo[d]benzo[4,5]imidazo[1,2-a]imidazole

: 1537905-39-7
5-(9H-carbazol-3-yl)benzimidazolo[1,2-a]benzimidazole

: 1537905-21-7
C₄₄H₂₇N₇

Guidance literature:: With copper(l) iodide; potassium phosphate monohydrate; trans-1,2-Diaminocyclohexane; In 1,4-dioxane; for 6h; Reflux; Inert atmosphere;

Reference yield:

: 28890-99-5
benzimidazolo<1,2-a>benzimidazole

: 1537905-21-7
C₄₄H₂₇N₇

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; caesium carbonate; L-proline / dimethyl sulfoxide / 26 h / 120 °C / Inert atmosphere

2: [bis(acetoxy)iodo]benzene; iodine / 28 h / 25 °C

3: copper(l) iodide; potassium phosphate monohydrate; trans-1,2-Diaminocyclohexane / 1,4-dioxane / 6 h / Reflux; Inert atmosphere

With copper(l) iodide; potassium phosphate monohydrate; [bis(acetoxy)iodo]benzene; trans-1,2-Diaminocyclohexane; iodine; caesium carbonate; L-proline; In 1,4-dioxane; dimethyl sulfoxide;

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 1537905-21-7
C₄₄H₂₇N₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-iodo-succinimide; acetic acid / 5 h / 20 °C / Inert atmosphere

2.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

2.2: 2 h / 20 - 50 °C

3.1: copper(l) iodide; potassium phosphate monohydrate; trans-1,2-Diaminocyclohexane / 1,4-dioxane / 48 h / 100 °C / Inert atmosphere

4.1: potassium hydroxide / ethanol / 5 h / Inert atmosphere

5.1: copper(l) iodide; potassium phosphate monohydrate; trans-1,2-Diaminocyclohexane / 1,4-dioxane / 6 h / Reflux; Inert atmosphere

With N-iodo-succinimide; copper(l) iodide; potassium phosphate monohydrate; trans-1,2-Diaminocyclohexane; sodium hydride; acetic acid; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; mineral oil;