(β-phenylethynyl)pentafluorocyclotriphosphazene

Base Information

Chemical Name:(β-phenylethynyl)pentafluorocyclotriphosphazene
CAS No.:34671-22-2
Molecular Formula:C₈H₅F₅N₃P₃
Molecular Weight:331.061
Hs Code.:

Synonyms:(β-phenylethynyl)pentafluorocyclotriphosphazene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (β-phenylethynyl)pentafluorocyclotriphosphazene

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Technology Process of (β-phenylethynyl)pentafluorocyclotriphosphazene

There total 1 articles about (β-phenylethynyl)pentafluorocyclotriphosphazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 536-74-3
phenylacetylene

: 34671-22-2
(β-phenylethynyl)pentafluorocyclotriphosphazene

Guidance literature:: With n-butyllithium; hexafluorophosphazene; Yield given. Multistep reaction; 1.) ether, 24 h, 2.) ether, 24 h;

Reference yield: 87.0%

: 34671-22-2
(β-phenylethynyl)pentafluorocyclotriphosphazene

: Ph(CH₂)2P₃N₃F₅

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 2h; Schlenk technique;
DOI:10.1016/j.jfluchem.2014.07.022

Reference yield: 27.0%

: η5-carbomethoxycyclopentadienyl(η4-cyclooctadiene)cobalt

: 34671-22-2
(β-phenylethynyl)pentafluorocyclotriphosphazene

: 536-74-3
phenylacetylene

: 912478-05-8
[η5-carboxymethoxycyclopentadienyl][η4-1,3-bis(pentafluorocycltriphosphazenyl)-2,4-diphenylcyclobutadiene]cobalt

: η5-carbomethoxycyclopentadienyl(η4-1-mono(pentafluorocyclotriphosphazene)-2,3-diphenyl-4a,5,6,9,10,10a-hexahydro[8]annulene)cobalt

Guidance literature:: In xylene; byproducts: 1,3,5-triphenylbenzene, 1,2,4-triphenylbenzene, (pentafluorocyclotriphosphazenyl)triphenylbenzene; under N2; soln. of Co complex, PhC2P3N3F5 and PhCCH in xylene refluxed for 33 h; solvent evapd.; column chromy. (silica gel, hexane to hexane/ethylacetate (6%)); elem. anal.;
DOI:10.1021/ic7024507