(η5-carboxymethoxycyclopentadienyl)(triphenylphosphine)-2,5-bis(pentafluorocyclotriphosphazenyl)-3,4-diphenyl cobaltacyclopentadiene

Base Information

Chemical Name:(η5-carboxymethoxycyclopentadienyl)(triphenylphosphine)-2,5-bis(pentafluorocyclotriphosphazenyl)-3,4-diphenyl cobaltacyclopentadiene
CAS No.:912478-03-6
Molecular Formula:C₄₁H₃₂CoF₁₀N₆O₂P₇
Molecular Weight:1106.54
Hs Code.:

(η5-carboxymethoxycyclopentadienyl)(triphenylphosphine)-2,5-bis(pentafluorocyclotriphosphazenyl)-3,4-diphenyl cobaltacyclopentadiene

Synonyms:(η5-carboxymethoxycyclopentadienyl)(triphenylphosphine)-2,5-bis(pentafluorocyclotriphosphazenyl)-3,4-diphenyl cobaltacyclopentadiene

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Chemical Property of (η5-carboxymethoxycyclopentadienyl)(triphenylphosphine)-2,5-bis(pentafluorocyclotriphosphazenyl)-3,4-diphenyl cobaltacyclopentadiene

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Technology Process of (η5-carboxymethoxycyclopentadienyl)(triphenylphosphine)-2,5-bis(pentafluorocyclotriphosphazenyl)-3,4-diphenyl cobaltacyclopentadiene

There total 1 articles about (η5-carboxymethoxycyclopentadienyl)(triphenylphosphine)-2,5-bis(pentafluorocyclotriphosphazenyl)-3,4-diphenyl cobaltacyclopentadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 26305-75-9
chlorotris(triphenylphosphine)cobalt(I)

: 34671-22-2
(β-phenylethynyl)pentafluorocyclotriphosphazene

: sodium (methoxycarbonyl)cyclopentadienide

: 912478-05-8
[η5-carboxymethoxycyclopentadienyl][η4-1,3-bis(pentafluorocycltriphosphazenyl)-2,4-diphenylcyclobutadiene]cobalt

: 912478-04-7
(η5-carboxymethoxycyclopentadienyl)(triphenylphosphine)-2,4-bis(pentafluorocyclotriphosphazenyl)-3,5-diphenyl cobaltacyclopentadiene

: 912478-03-6
(η5-carboxymethoxycyclopentadienyl)(triphenylphosphine)-2,5-bis(pentafluorocyclotriphosphazenyl)-3,4-diphenyl cobaltacyclopentadiene

Guidance literature:: In tetrahydrofuran; toluene; byproducts: triphenylphosphine, triphenylphosphine oxide; (N2); addn. of a soln. of phosphorus compd. and cobalt complex in toluene to a soln. of ligand in THF, stirring at room temp. for 15 min, refluxfor 24 h; evapn., column chromy. (silica gel, hexane, then 2%, then 2.5%, then 3% ethyl acetate in hexane); elem. anal.;
DOI:10.1021/ic0609204

Reference yield: 25.0%

: 912478-03-6
(η5-carboxymethoxycyclopentadienyl)(triphenylphosphine)-2,5-bis(pentafluorocyclotriphosphazenyl)-3,4-diphenyl cobaltacyclopentadiene

: 501-65-5
diphenyl acetylene

: 182627-81-2
(η⁵-carbomethoxycyclopentadienyl)-(η⁴-tetraphenylcyclobutadiene)cobalt

Guidance literature:: In xylene; byproducts: triphenylphosphine, 1,4-bis(pentafluorocyclotriphosphazenyl)-C6Ph4; (N2); refluxing a soln. of cobalt complex and alkyne in xylene for 24 h; evapn. in vac., column chromy. (silica gel, hexane, then 2%, then 5% ethyl acetate in hexane);
DOI:10.1021/ic0609204