benzyl 4-hydroxy-2-(3'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

Base Information

Chemical Name:benzyl 4-hydroxy-2-(3'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate
CAS No.:141631-54-1
Molecular Formula:C₂₅H₂₄O₇
Molecular Weight:436.461
Hs Code.:

Synonyms:benzyl 4-hydroxy-2-(3'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

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Chemical Property of benzyl 4-hydroxy-2-(3'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

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Technology Process of benzyl 4-hydroxy-2-(3'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

There total 5 articles about benzyl 4-hydroxy-2-(3'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 100-39-0
benzyl bromide

: 141631-53-0
4-hydroxy-2-(3'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoic acid

: 141631-54-1
benzyl 4-hydroxy-2-(3'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 12h; Ambient temperature;

Reference yield:

: 61158-11-0
methyl 4-O-benzyllecanorate

: 141631-54-1
benzyl 4-hydroxy-2-(3'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / potassium carbonate / dimethylsulfoxide / 12 h / Ambient temperature

2: 91 percent / sodium hydrogen carbonate / dimethylformamide / 14 h / Ambient temperature

3: 97 percent / potassium carbonate / acetone / 18 h / Heating

4: 99 percent / H₂ / 10percent Pd/C / ethyl acetate / 16 h

5: 97 percent / sodium hydrogen carbonate / dimethylformamide / 12 h / Ambient temperature

With hydrogen; sodium hydrogencarbonate; potassium carbonate; palladium on activated charcoal; In dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone;

Reference yield:

: 111699-18-4
4-benzyloxy-2-(3'-hydroxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoic acid

: 141631-54-1
benzyl 4-hydroxy-2-(3'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / sodium hydrogen carbonate / dimethylformamide / 14 h / Ambient temperature

2: 97 percent / potassium carbonate / acetone / 18 h / Heating

3: 99 percent / H₂ / 10percent Pd/C / ethyl acetate / 16 h

4: 97 percent / sodium hydrogen carbonate / dimethylformamide / 12 h / Ambient temperature

With hydrogen; sodium hydrogencarbonate; potassium carbonate; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide; acetone;