N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

Base Information

Chemical Name:N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester
CAS No.:97857-37-9
Molecular Formula:C₄₆H₅₅N₅O₁₀
Molecular Weight:837.97
Hs Code.:

Synonyms:N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

Suppliers and Price of N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

There total 5 articles about N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 57471-71-3
N^α-Z-glycyl-L-phenylalanyl-L-phenylalanine

: 97857-36-8
O-tert-butyl-L-tyrosyl-L-threonine methyl ester

: 97857-37-9
N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at -10 - -5 ℃; for 3.5h; then 48 h at 20 deg C;

Reference yield:

: 5545-54-0
N-(benzyloxycarbonyl)-O-(1,1-dimethylethyl)-L-tyrosine

: 97857-37-9
N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 72.7 percent / triethylamine, 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide; tetrahydrofuran / 1 h / 0 °C / then 24 h at 20 deg C

2: 100 percent / hydrogen / palladium black / methanol / 5 h / 20 °C / 760 Torr

3: 52 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide / 3.5 h / -10 - -5 °C / then 48 h at 20 deg C

With hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 73116-15-1
N-Z-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

: 97857-37-9
N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / hydrogen / palladium black / methanol / 5 h / 20 °C / 760 Torr

2: 52 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide / 3.5 h / -10 - -5 °C / then 48 h at 20 deg C

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium; In methanol; N,N-dimethyl-formamide;