N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine

Base Information

Chemical Name:N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine
CAS No.:73116-17-3
Molecular Formula:C₄₅H₅₃N₅O₁₀
Molecular Weight:823.943
Hs Code.:

Synonyms:N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine

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Technology Process of N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine

There total 7 articles about N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 97857-37-9
N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

: 73116-17-3
N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine

Guidance literature:: With sodium hydroxide; In methanol; water; at 20 ℃; for 3h;

Reference yield:

: 5545-54-0
N-(benzyloxycarbonyl)-O-(1,1-dimethylethyl)-L-tyrosine

: 73116-17-3
N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine

Guidance literature:: Multi-step reaction with 4 steps

1: 72.7 percent / triethylamine, 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide; tetrahydrofuran / 1 h / 0 °C / then 24 h at 20 deg C

2: 100 percent / hydrogen / palladium black / methanol / 5 h / 20 °C / 760 Torr

3: 52 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide / 3.5 h / -10 - -5 °C / then 48 h at 20 deg C

4: 88 percent / 2 N NaOH / methanol; H₂O / 3 h / 20 °C

With sodium hydroxide; hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 73116-15-1
N-Z-O-tert-butyl-L-tyrosyl-L-threonine methyl ester

: 73116-17-3
N-Z-glycyl-L-phenylalanyl-L-phenylalanyl-O-tert-butyl-L-tyrosyl-L-threonine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / hydrogen / palladium black / methanol / 5 h / 20 °C / 760 Torr

2: 52 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide / 3.5 h / -10 - -5 °C / then 48 h at 20 deg C

3: 88 percent / 2 N NaOH / methanol; H₂O / 3 h / 20 °C

With sodium hydroxide; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium; In methanol; water; N,N-dimethyl-formamide;