carbamic acid, [(5-bromo-2-hydroxyphenyl)methyl](2-hydroxy

Base Information

Chemical Name:carbamic acid, [(5-bromo-2-hydroxyphenyl)methyl](2-hydroxy
CAS No.:1217862-54-8
Molecular Formula:C₁₄H₂₀BrNO₄
Molecular Weight:346.221
Hs Code.:
Mol file:1217862-54-8.mol

Synonyms:tert-butyl N-(5-bromo-2-hydroxybenzyl)-N-(2-hydroxyethyl)carbamate

Suppliers and Price of carbamic acid, [(5-bromo-2-hydroxyphenyl)methyl](2-hydroxy

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
tert-Butyl (5-bromo-2-hydroxybenzyl)-(2-hydroxyethyl)carbamate
500mg
$ 158.00

Crysdot
tert-Butyl5-bromo-2-hydroxybenzyl(2-hydroxyethyl)carbamate 97%
5g
$ 757.00

Total 3 raw suppliers

Chemical Property of carbamic acid, [(5-bromo-2-hydroxyphenyl)methyl](2-hydroxy

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl (5-bromo-2-hydroxybenzyl)-(2-hydroxyethyl)carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of carbamic acid, [(5-bromo-2-hydroxyphenyl)methyl](2-hydroxy

There total 4 articles about carbamic acid, [(5-bromo-2-hydroxyphenyl)methyl](2-hydroxy which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 141-43-5
ethanolamine

: 1761-61-1
5-bromosalicyclaldehyde

: 1217862-54-8
tert-butyl N-(5-bromo-2-hydroxybenzyl)-N-(2-hydroxyethyl)carbamate

Guidance literature:: ethanolamine; 5-bromosalicyclaldehyde; With methanol; sodium tetrahydroborate; In tetrahydrofuran; at 40 ℃; for 4h;

di-tert-butyl dicarbonate; With sodium hydrogencarbonate; In water; ethyl acetate; at 20 ℃;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1181407-01-1
C₉H₁₂BrNO₂

: 1217862-54-8
tert-butyl N-(5-bromo-2-hydroxybenzyl)-N-(2-hydroxyethyl)carbamate

Guidance literature:: With sodium hydrogencarbonate; In water; ethyl acetate; at 20 ℃;

Reference yield:

: 21974-51-6
4-bromo-2-[(2-hydroxyethyl)-iminomethyl]phenol

: 1217862-54-8
tert-butyl N-(5-bromo-2-hydroxybenzyl)-N-(2-hydroxyethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 0.5 h

2: sodium hydroxide / methanol / 1 h

With sodium tetrahydroborate; sodium hydroxide; In methanol;
DOI:10.1021/jm3007933