benzyl 3,4,5-tribenzyloxy-2-(5-tert-butoxycarbonyl-2,3-dihydroxyphenoxy)benzoate

Base Information

Chemical Name:benzyl 3,4,5-tribenzyloxy-2-(5-tert-butoxycarbonyl-2,3-dihydroxyphenoxy)benzoate
CAS No.:1606148-53-1
Molecular Formula:C₄₆H₄₂O₁₀
Molecular Weight:754.833
Hs Code.:

Synonyms:benzyl 3,4,5-tribenzyloxy-2-(5-tert-butoxycarbonyl-2,3-dihydroxyphenoxy)benzoate

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Chemical Property of benzyl 3,4,5-tribenzyloxy-2-(5-tert-butoxycarbonyl-2,3-dihydroxyphenoxy)benzoate

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Technology Process of benzyl 3,4,5-tribenzyloxy-2-(5-tert-butoxycarbonyl-2,3-dihydroxyphenoxy)benzoate

There total 7 articles about benzyl 3,4,5-tribenzyloxy-2-(5-tert-butoxycarbonyl-2,3-dihydroxyphenoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1606148-52-0
benzyl 2-(2,3-benzaloxy-5-tert-butoxycarbonylphenoxy)-3,4,5-tribenzyloxybenzoate

: 1606148-53-1
benzyl 3,4,5-tribenzyloxy-2-(5-tert-butoxycarbonyl-2,3-dihydroxyphenoxy)benzoate

Guidance literature:: With ethanethiol; tin(ll) chloride; In dichloromethane; at 0 - 20 ℃; for 22h;
DOI:10.1248/cpb.c13-00458

Reference yield:

: 149-91-7
3,4,5-trihydroxybenzoic acid

: 1606148-53-1
benzyl 3,4,5-tribenzyloxy-2-(5-tert-butoxycarbonyl-2,3-dihydroxyphenoxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 0 - 20 °C / Inert atmosphere

2: pyridine / 8 h / 110 °C / Inert atmosphere

3: copper / N,N-dimethyl acetamide / 0.5 h / 160 °C / Inert atmosphere

4: tin(ll) chloride; ethanethiol / dichloromethane / 22 h / 0 - 20 °C

With pyridine; sulfuric acid; copper; ethanethiol; tin(ll) chloride; In dichloromethane; N,N-dimethyl acetamide;
DOI:10.1248/cpb.c13-00458

Reference yield:

: 1606148-51-9
tert-butyl 3,4-benzaloxy-5-hydroxybenzoate

: 1606148-53-1
benzyl 3,4,5-tribenzyloxy-2-(5-tert-butoxycarbonyl-2,3-dihydroxyphenoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: copper / N,N-dimethyl acetamide / 0.5 h / 160 °C / Inert atmosphere

2: tin(ll) chloride; ethanethiol / dichloromethane / 22 h / 0 - 20 °C

With copper; ethanethiol; tin(ll) chloride; In dichloromethane; N,N-dimethyl acetamide;
DOI:10.1248/cpb.c13-00458