benzyl 2-(2,3-benzaloxy-5-tert-butoxycarbonylphenoxy)-3,4,5-tribenzyloxybenzoate

Base Information

Chemical Name:benzyl 2-(2,3-benzaloxy-5-tert-butoxycarbonylphenoxy)-3,4,5-tribenzyloxybenzoate
CAS No.:1606148-52-0
Molecular Formula:C₅₃H₄₆O₁₀
Molecular Weight:842.942
Hs Code.:

Synonyms:benzyl 2-(2,3-benzaloxy-5-tert-butoxycarbonylphenoxy)-3,4,5-tribenzyloxybenzoate

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Chemical Property of benzyl 2-(2,3-benzaloxy-5-tert-butoxycarbonylphenoxy)-3,4,5-tribenzyloxybenzoate

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Technology Process of benzyl 2-(2,3-benzaloxy-5-tert-butoxycarbonylphenoxy)-3,4,5-tribenzyloxybenzoate

There total 5 articles about benzyl 2-(2,3-benzaloxy-5-tert-butoxycarbonylphenoxy)-3,4,5-tribenzyloxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149-91-7
3,4,5-trihydroxybenzoic acid

: 1606148-52-0
benzyl 2-(2,3-benzaloxy-5-tert-butoxycarbonylphenoxy)-3,4,5-tribenzyloxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 0 - 20 °C / Inert atmosphere

2: pyridine / 8 h / 110 °C / Inert atmosphere

3: copper / N,N-dimethyl acetamide / 0.5 h / 160 °C / Inert atmosphere

With pyridine; sulfuric acid; copper; In N,N-dimethyl acetamide;
DOI:10.1248/cpb.c13-00458

Reference yield:

: 475161-97-8
benzyl 3,4,5-tris(benzyloxy)benzoate

: 1606148-52-0
benzyl 2-(2,3-benzaloxy-5-tert-butoxycarbonylphenoxy)-3,4,5-tribenzyloxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 24 h / 20 °C

2: copper / N,N-dimethyl acetamide / 0.5 h / 160 °C / Inert atmosphere

With N-Bromosuccinimide; copper; In N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1248/cpb.c13-00458

Reference yield:

: 100-44-7
benzyl chloride

: 1606148-52-0
benzyl 2-(2,3-benzaloxy-5-tert-butoxycarbonylphenoxy)-3,4,5-tribenzyloxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 4.5 h / 100 °C

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 24 h / 20 °C

3: copper / N,N-dimethyl acetamide / 0.5 h / 160 °C / Inert atmosphere

With N-Bromosuccinimide; tetra-(n-butyl)ammonium iodide; copper; potassium carbonate; In N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1248/cpb.c13-00458