Technology Process of Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate
There total 15 articles about Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 39 percent / pyridine / 12 h / Ambient temperature
2: 98 percent / K2CO3 / methanol / 1 h / Ambient temperature
3: 58 percent / molecular sieves 3 Angstroem, propionic acid / 48 h / 130 °C
With
pyridine; 3 A molecular sieve; potassium carbonate; propionic acid;
In
methanol;
DOI:10.1039/a604365h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / K2CO3 / methanol / 1 h / Ambient temperature
2: 1.) PPh3, benzoic acid, diethyl azodicarboxylate, 2.) K2CO3 / 1.) Et2O, r.t., 30 min, 2.) MeOH, r.t., 2 h
3: 58 percent / molecular sieves 3 Angstroem, propionic acid / 48 h / 130 °C
With
3 A molecular sieve; potassium carbonate; propionic acid; triphenylphosphine; benzoic acid; diethylazodicarboxylate;
In
methanol;
DOI:10.1039/a604365h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 98 percent / K2CO3 / methanol / 1 h / Ambient temperature
2: 58 percent / molecular sieves 3 Angstroem, propionic acid / 48 h / 130 °C
With
3 A molecular sieve; potassium carbonate; propionic acid;
In
methanol;
DOI:10.1039/a604365h