Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate

Base Information

Chemical Name:Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate
CAS No.:156487-78-4
Molecular Formula:C₂₀H₂₈O₆
Molecular Weight:364.439
Hs Code.:

Synonyms:Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate

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Technology Process of Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate

There total 15 articles about Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-3-(3,4-Dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enol

: 156487-78-4
Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 39 percent / pyridine / 12 h / Ambient temperature

2: 98 percent / K₂CO₃ / methanol / 1 h / Ambient temperature

3: 58 percent / molecular sieves 3 Angstroem, propionic acid / 48 h / 130 °C

With pyridine; 3 A molecular sieve; potassium carbonate; propionic acid; In methanol;
DOI:10.1039/a604365h

Reference yield:

: 187277-52-7
Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

: 156487-78-4
Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / K₂CO₃ / methanol / 1 h / Ambient temperature

2: 1.) PPh₃, benzoic acid, diethyl azodicarboxylate, 2.) K₂CO₃ / 1.) Et₂O, r.t., 30 min, 2.) MeOH, r.t., 2 h

3: 58 percent / molecular sieves 3 Angstroem, propionic acid / 48 h / 130 °C

With 3 A molecular sieve; potassium carbonate; propionic acid; triphenylphosphine; benzoic acid; diethylazodicarboxylate; In methanol;
DOI:10.1039/a604365h

Reference yield:

: 187277-51-6
Acetic acid (1R,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

: 156487-78-4
Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / K₂CO₃ / methanol / 1 h / Ambient temperature

2: 58 percent / molecular sieves 3 Angstroem, propionic acid / 48 h / 130 °C

With 3 A molecular sieve; potassium carbonate; propionic acid; In methanol;
DOI:10.1039/a604365h