2-acetamido-3,6-di-O-acetyl-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

Base Information

Chemical Name:2-acetamido-3,6-di-O-acetyl-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol
CAS No.:1227636-91-0
Molecular Formula:C₂₆H₃₂N₂O₆
Molecular Weight:468.55
Hs Code.:

Synonyms:2-acetamido-3,6-di-O-acetyl-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

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Chemical Property of 2-acetamido-3,6-di-O-acetyl-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

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Technology Process of 2-acetamido-3,6-di-O-acetyl-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

There total 5 articles about 2-acetamido-3,6-di-O-acetyl-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1227636-89-6
3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

: 108-24-7
acetic anhydride

: 1227636-91-0
2-acetamido-3,6-di-O-acetyl-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

Guidance literature:: With copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.201200110

Reference yield:

: 1401914-18-8
methyl-5-azido-3-O-benzyl-5-deoxy-L-talofuranoside

: 1227636-91-0
2-acetamido-3,6-di-O-acetyl-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / dichloromethane

2: tetrahydrofuran

3: boron trifluoride diethyl etherate

4: diisobutylaluminium hydride; pyridine / dichloromethane

5: acetic acid; copper(II) sulfate / zinc / tetrahydrofuran

With pyridine; boron trifluoride diethyl etherate; diisobutylaluminium hydride; copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; dichloromethane;

Reference yield:

: C₁₆H₁₇F₆N₃O₉S₂

: 1227636-91-0
2-acetamido-3,6-di-O-acetyl-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran

2: boron trifluoride diethyl etherate

3: diisobutylaluminium hydride; pyridine / dichloromethane

4: acetic acid; copper(II) sulfate / zinc / tetrahydrofuran

With pyridine; boron trifluoride diethyl etherate; diisobutylaluminium hydride; copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; dichloromethane;