1N-methyl-2-acetamido-1,2,5-trideoxy-1,5-imino-D-galactitol

Base Information

Chemical Name:1N-methyl-2-acetamido-1,2,5-trideoxy-1,5-imino-D-galactitol
CAS No.:1401914-31-5
Molecular Formula:C₉H₁₈N₂O₄
Molecular Weight:218.253
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1N-methyl-2-acetamido-1,2,5-trideoxy-1,5-imino-D-galactitol

Chemical Property:

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Technology Process of 1N-methyl-2-acetamido-1,2,5-trideoxy-1,5-imino-D-galactitol

There total 9 articles about 1N-methyl-2-acetamido-1,2,5-trideoxy-1,5-imino-D-galactitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 105265-96-1,105615-44-9,117894-14-1,133697-32-2
N-((3S,4R,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)piperidin-3-yl)acetamide

: 1401914-31-5
1N-methyl-2-acetamido-1,2,5-trideoxy-1,5-imino-D-galactitol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In 1,4-dioxane; water; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1002/chem.201200110

Reference yield:

: 1401914-18-8
methyl-5-azido-3-O-benzyl-5-deoxy-L-talofuranoside

: 1401914-31-5
1N-methyl-2-acetamido-1,2,5-trideoxy-1,5-imino-D-galactitol

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridine / dichloromethane / 1 h / -40 °C / Inert atmosphere

2.1: tetrahydrofuran / 2 h / -30 - 20 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate; acetic anhydride / 2.5 h / -30 - 20 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.75 h / -78 °C / Inert atmosphere

4.2: 3 h / 0 - 20 °C / Inert atmosphere

4.3: 16 h / 20 °C / Inert atmosphere

5.1: copper(II) sulfate; acetic acid; zinc / tetrahydrofuran / 0.5 h / Inert atmosphere

6.1: sodium methylate / methanol / 16 h / 20 °C / Inert atmosphere

7.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / water / 24 h / 20 °C / Inert atmosphere

8.1: Dowex (50W-X₈, H⁺) / water / Inert atmosphere

9.1: palladium 10% on activated carbon; hydrogen / 1,4-dioxane; water / 18 h / 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; sodium methylate; acetic anhydride; diisobutylaluminium hydride; copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene;
DOI:10.1002/chem.201200110

Reference yield:

: C₁₆H₁₇F₆N₃O₉S₂

: 1401914-31-5
1N-methyl-2-acetamido-1,2,5-trideoxy-1,5-imino-D-galactitol

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran / 2 h / -30 - 20 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate; acetic anhydride / 2.5 h / -30 - 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.75 h / -78 °C / Inert atmosphere

3.2: 3 h / 0 - 20 °C / Inert atmosphere

3.3: 16 h / 20 °C / Inert atmosphere

4.1: copper(II) sulfate; acetic acid; zinc / tetrahydrofuran / 0.5 h / Inert atmosphere

5.1: sodium methylate / methanol / 16 h / 20 °C / Inert atmosphere

6.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / water / 24 h / 20 °C / Inert atmosphere

7.1: Dowex (50W-X₈, H⁺) / water / Inert atmosphere

8.1: palladium 10% on activated carbon; hydrogen / 1,4-dioxane; water / 18 h / 20 °C / Inert atmosphere

With hydrogenchloride; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; sodium methylate; acetic anhydride; diisobutylaluminium hydride; copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene;
DOI:10.1002/chem.201200110