3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

Base Information

Chemical Name:3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol
CAS No.:1227636-89-6
Molecular Formula:C₂₄H₂₈N₄O₅
Molecular Weight:452.51
Hs Code.:

Synonyms:3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

Suppliers and Price of 3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

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Technology Process of 3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

There total 12 articles about 3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: C₂₅H₃₀N₄O₆

: 108-24-7
acetic anhydride

: 1227636-89-6
3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

Guidance literature:: C₂₅H₃₀N₄O₆; With diisobutylaluminium hydride; In dichloromethane;

With sodium tetrahydroborate; In methanol;

acetic anhydride; With pyridine;
DOI:10.1016/j.tetlet.2010.02.063

Reference yield:

: 1227636-87-4
4-O-acetyl-5-azido-2-N,3-O-dibenzyl-2,5,6-trideoxy-2,6-imino-L-galactose acetyl methyl acetal

: 1227636-89-6
3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

Guidance literature:: 4-O-acetyl-5-azido-2-N,3-O-dibenzyl-2,5,6-trideoxy-2,6-imino-L-galactose acetyl methyl acetal; With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 0.75h; Inert atmosphere;

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 3h; Inert atmosphere;

With pyridine; acetic anhydride; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.201200110

Reference yield:

: 1401914-18-8
methyl-5-azido-3-O-benzyl-5-deoxy-L-talofuranoside

: 1227636-89-6
3,6-di-O-acetyl-2-azido-1-N,4-O-dibenzyl-1,2,5-trideoxy-1,5-imino-D-galactitol

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane

2: tetrahydrofuran

3: boron trifluoride diethyl etherate

4: diisobutylaluminium hydride; pyridine / dichloromethane

With pyridine; boron trifluoride diethyl etherate; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane;