2,5-di-(1,3,2-dithiarsolan-2yl)-9(4-fluorophenyl)-6[14C]methoxy-3-fluorone

Base Information

Chemical Name:2,5-di-(1,3,2-dithiarsolan-2yl)-9(4-fluorophenyl)-6[14C]methoxy-3-fluorone
CAS No.:1378318-69-4
Molecular Formula:C₂₄H₁₉As₂FO₃S₄
Molecular Weight:654.508
Hs Code.:

Synonyms:2,5-di-(1,3,2-dithiarsolan-2yl)-9(4-fluorophenyl)-6[14C]methoxy-3-fluorone

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Chemical Property of 2,5-di-(1,3,2-dithiarsolan-2yl)-9(4-fluorophenyl)-6[14C]methoxy-3-fluorone

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Technology Process of 2,5-di-(1,3,2-dithiarsolan-2yl)-9(4-fluorophenyl)-6[14C]methoxy-3-fluorone

There total 7 articles about 2,5-di-(1,3,2-dithiarsolan-2yl)-9(4-fluorophenyl)-6[14C]methoxy-3-fluorone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16170-82-4
[14C]methyl iodide

: 1378318-62-7
2,5-di-(1,3,2-dithiarsolan-2-yl)-9-(4-fluorophenyl)-6-hydroxy-3-fluorone

: 1378318-69-4
2,5-di-(1,3,2-dithiarsolan-2yl)-9(4-fluorophenyl)-6[14C]methoxy-3-fluorone

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 17715-69-4
1-Bromo-2,4-dimethoxybenzene

: 1378318-69-4
2,5-di-(1,3,2-dithiarsolan-2yl)-9(4-fluorophenyl)-6[14C]methoxy-3-fluorone

Guidance literature:: Multi-step reaction with 5 steps

1.1: iodine; magnesium / tetrahydrofuran / 0.5 h

2.1: boron tribromide / dichloromethane / -78 - 20 °C

4.1: N-ethyl-N,N-diisopropylamine / palladium diacetate / 1-methyl-pyrrolidin-2-one / 22 - 55 °C / Inert atmosphere

4.2: 0.5 h / pH 6.9 / Aqueous phosphate buffer

5.1: N,N-dimethyl-formamide / 20 °C

With iodine; boron tribromide; magnesium; N-ethyl-N,N-diisopropylamine; palladium diacetate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1378318-45-6
bis(2,4-dimethoxyphenyl)-4-fluorophenyl methanol

: 1378318-69-4
2,5-di-(1,3,2-dithiarsolan-2yl)-9(4-fluorophenyl)-6[14C]methoxy-3-fluorone

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron tribromide / dichloromethane / -78 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine / palladium diacetate / 1-methyl-pyrrolidin-2-one / 22 - 55 °C / Inert atmosphere

3.2: 0.5 h / pH 6.9 / Aqueous phosphate buffer

4.1: N,N-dimethyl-formamide / 20 °C

With boron tribromide; N-ethyl-N,N-diisopropylamine; palladium diacetate; In 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide;