3-hydroxymethyl-5-methylbenzoic acid

Base Information

Chemical Name:3-hydroxymethyl-5-methylbenzoic acid
CAS No.:63440-59-5
Molecular Formula:C₉H₁₀O₃
Molecular Weight:166.177
Hs Code.:

Synonyms:3-hydroxymethyl-5-methylbenzoic acid

Suppliers and Price of 3-hydroxymethyl-5-methylbenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-hydroxymethyl-5-methylbenzoic acid

Chemical Property:

Boiling Point:361.2±30.0 °C(Predicted)
Density:1.258±0.06 g/cm3(Predicted)

Purity/Quality:: 98%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 3-Methyl-5-hydroxymethylbenzoic Acid is an intermediate in the synthesis of RH 9886 (R315770), a pesticide derivative of Tebufenozide (T013200) is a synthetic nonsteroidal ecdysone agonist used in pesticide formulations (1) that causes premature molting; novel insect growth regulator (2,3,4) specific to lepidopteran species. Drinking water Contaminant Candidate List 3 (CCL3) as per United States Environmental Protection Agency (EPA). Environmental contaminants; Food contaminants.

Technology Process of 3-hydroxymethyl-5-methylbenzoic acid

There total 3 articles about 3-hydroxymethyl-5-methylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 550367-75-4
3-bromomethyl-5-methylbenzoic acid

: 4481-27-0
3-formyl-5-methylbenzoic acid

: 63440-59-5
3-hydroxymethyl-5-methylbenzoic acid

Guidance literature:: With copper nitrate hemi(pentahydrate); In water; acetonitrile; for 2h; Reflux;
DOI:10.1016/j.ejmech.2016.03.048

Reference yield:

: 499-06-9
3,5-dimethylbenzoic acid

: 63440-59-5
3-hydroxymethyl-5-methylbenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / dichloromethane / 18 h / Reflux

2: copper nitrate hemi(pentahydrate) / acetonitrile; water / 2 h / Reflux

With N-Bromosuccinimide; copper nitrate hemi(pentahydrate); 2,2'-azobis(isobutyronitrile); In dichloromethane; water; acetonitrile;
DOI:10.1016/j.ejmech.2016.03.048