N-(4'-tert-butoxycarbonylbenzyl)-N,N-dimethyl-N-{1-[(-)-8-phenylmenthyloxycarbonylbut-3-en-1-yl]}ammonium bromide

Base Information

Chemical Name:N-(4'-tert-butoxycarbonylbenzyl)-N,N-dimethyl-N-{1-[(-)-8-phenylmenthyloxycarbonylbut-3-en-1-yl]}ammonium bromide
CAS No.:1088482-15-8
Molecular Formula:Br*C₃₅H₅₀NO₄
Molecular Weight:628.69
Hs Code.:

Synonyms:N-(4'-tert-butoxycarbonylbenzyl)-N,N-dimethyl-N-{1-[(-)-8-phenylmenthyloxycarbonylbut-3-en-1-yl]}ammonium bromide

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Chemical Property of N-(4'-tert-butoxycarbonylbenzyl)-N,N-dimethyl-N-{1-[(-)-8-phenylmenthyloxycarbonylbut-3-en-1-yl]}ammonium bromide

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Technology Process of N-(4'-tert-butoxycarbonylbenzyl)-N,N-dimethyl-N-{1-[(-)-8-phenylmenthyloxycarbonylbut-3-en-1-yl]}ammonium bromide

There total 1 articles about N-(4'-tert-butoxycarbonylbenzyl)-N,N-dimethyl-N-{1-[(-)-8-phenylmenthyloxycarbonylbut-3-en-1-yl]}ammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1088482-13-6
2-dimethylaminopent-4-enoic acid (-)-8-phenylmenthol ester

: 108052-76-2
4-(bromomethyl)benzoic acid 1,1-dimethylethyl ester

: 1088482-15-8
N-(4'-tert-butoxycarbonylbenzyl)-N,N-dimethyl-N-{1-[(-)-8-phenylmenthyloxycarbonylbut-3-en-1-yl]}ammonium bromide

Guidance literature:: In acetonitrile; at 20 ℃; for 48h; optical yield given as %de;
DOI:10.1039/b811162f

Reference yield: 36.0%

: 1088482-15-8
N-(4'-tert-butoxycarbonylbenzyl)-N,N-dimethyl-N-{1-[(-)-8-phenylmenthyloxycarbonylbut-3-en-1-yl]}ammonium bromide

: 1088482-17-0
2-(4'-tert-butoxycarbonylbenzyl)-2-dimethylaminopent-4-enoic acid (-)-8-phenylmenthol ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -60 ℃; for 8h; optical yield given as %de; diastereoselective reaction;
DOI:10.1039/b811162f

Reference yield:

: 1088482-15-8
N-(4'-tert-butoxycarbonylbenzyl)-N,N-dimethyl-N-{1-[(-)-8-phenylmenthyloxycarbonylbut-3-en-1-yl]}ammonium bromide

: 1088481-68-8
(2S)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester

: 1088481-66-6
(2R)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-dimethylamino-4-enoic acid (-)-8-phenylmenthol ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -60 ℃; for 8h; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/b811162f