3-(5-(3,5-dichloro-4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)-4-iodobenzene-1-sulfonyl fluoride

Base Information

Chemical Name:3-(5-(3,5-dichloro-4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)-4-iodobenzene-1-sulfonyl fluoride
CAS No.:1422570-77-1
Molecular Formula:C₁₅H₈Cl₂FIN₂O₄S
Molecular Weight:529.114
Hs Code.:

Synonyms:3-(5-(3,5-dichloro-4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)-4-iodobenzene-1-sulfonyl fluoride

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Chemical Property of 3-(5-(3,5-dichloro-4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)-4-iodobenzene-1-sulfonyl fluoride

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Technology Process of 3-(5-(3,5-dichloro-4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)-4-iodobenzene-1-sulfonyl fluoride

There total 8 articles about 3-(5-(3,5-dichloro-4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)-4-iodobenzene-1-sulfonyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₀Cl₂FIN₂O₅S

: 1422570-77-1
3-(5-(3,5-dichloro-4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)-4-iodobenzene-1-sulfonyl fluoride

Guidance literature:: With dmap; p-toluenesulfonyl chloride; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/ja311729d

Reference yield:

: 850453-87-1
5-(chlorosulfonyl)-2-iodobenzoic acid

: 1422570-77-1
3-(5-(3,5-dichloro-4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)-4-iodobenzene-1-sulfonyl fluoride

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydrogen bifluoride / 1,4-dioxane; water / 0.5 h / 20 °C / Inert atmosphere

2: thionyl chloride / 2 h / 75 °C / Inert atmosphere

3: triethylamine / dichloromethane; dimethyl sulfoxide / 0.33 h / 20 °C / Inert atmosphere

4: p-toluenesulfonyl chloride; dmap / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

With dmap; thionyl chloride; potassium hydrogen bifluoride; triethylamine; p-toluenesulfonyl chloride; In 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ja311729d

Reference yield:

: 1422570-55-5
5-(fluorosulfonyl)-2-iodobenzoic acid

: 1422570-77-1
3-(5-(3,5-dichloro-4-methoxyphenyl)-1,3,4-oxadiazol-2-yl)-4-iodobenzene-1-sulfonyl fluoride

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 2 h / 75 °C / Inert atmosphere

2: triethylamine / dichloromethane; dimethyl sulfoxide / 0.33 h / 20 °C / Inert atmosphere

3: p-toluenesulfonyl chloride; dmap / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

With dmap; thionyl chloride; triethylamine; p-toluenesulfonyl chloride; In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja311729d