5-(fluorosulfonyl)-2-iodobenzoic acid

Base Information

Chemical Name:5-(fluorosulfonyl)-2-iodobenzoic acid
CAS No.:1422570-55-5
Molecular Formula:C₇H₄FIO₄S
Molecular Weight:330.075
Hs Code.:

Synonyms:5-(fluorosulfonyl)-2-iodobenzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(fluorosulfonyl)-2-iodobenzoic acid

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Technology Process of 5-(fluorosulfonyl)-2-iodobenzoic acid

There total 2 articles about 5-(fluorosulfonyl)-2-iodobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 850453-87-1
5-(chlorosulfonyl)-2-iodobenzoic acid

: 1422570-55-5
5-(fluorosulfonyl)-2-iodobenzoic acid

Guidance literature:: With potassium hydrogen bifluoride; In 1,4-dioxane; water; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja311729d

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 1422570-55-5
5-(fluorosulfonyl)-2-iodobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / 1 h / 120 °C / Inert atmosphere

2: potassium hydrogen bifluoride / 1,4-dioxane; water / 0.5 h / 20 °C / Inert atmosphere

With chlorosulfonic acid; potassium hydrogen bifluoride; In 1,4-dioxane; water;
DOI:10.1021/ja311729d