4,4,5,5-Tetramethyl-2-(3-methylbut-1-enyl)-1,3,2-dioxaborolane

Base Information

Chemical Name:4,4,5,5-Tetramethyl-2-(3-methylbut-1-enyl)-1,3,2-dioxaborolane
CAS No.:177949-92-7
Molecular Formula:C₁₁H₂₁BO₂
Molecular Weight:196.098
Hs Code.:
European Community (EC) Number:847-665-0
Nikkaji Number:J730.115D

Synonyms:177949-92-7;4,4,5,5-TETRAMETHYL-2-(3-METHYLBUT-1-ENYL)-1,3,2-DIOXABOROLANE;4,4,5,5-tetramethyl-2-[(E)-3-methylbut-1-enyl]-1,3,2-dioxaborolane;(E)-4,4,5,5-tetramethyl-2-(3-methylbut-1-en-1-yl)-1,3,2-dioxaborolane;SCHEMBL5777457;SCHEMBL5777463;AT21851;CS-0133499;EN300-7435879;Z1255463917;4,4,5,5-TETRAMETHYL-2-[(1E)-3-METHYLBUT-1-EN-1-YL]-1,3,2-DIOXABOROLANE

Suppliers and Price of 4,4,5,5-Tetramethyl-2-(3-methylbut-1-enyl)-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4,4,5,5-Tetramethyl-2-(3-methylbut-1-enyl)-1,3,2-dioxaborolane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:196.1634601
Heavy Atom Count:14
Complexity:215

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C=CC(C)C
Isomeric SMILES:B1(OC(C(O1)(C)C)(C)C)/C=C/C(C)C

Technology Process of 4,4,5,5-Tetramethyl-2-(3-methylbut-1-enyl)-1,3,2-dioxaborolane

There total 1 articles about 4,4,5,5-Tetramethyl-2-(3-methylbut-1-enyl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187817-21-5
4,4,5,5-tetramethyl-2-(3-methylbut-3-en-1-yl)-1,3,2-dioxaborolane

: 177949-92-7
(E)-4,4,5,5-tetramethyl-2-(3-methylbut-1-en-1-yl)-1,3,2-dioxaborolane

: 141550-13-2
4,4,5,5-tetramethyl-2-(3-methylbut-2-enyl)-1,3,2-dioxaborolane

Guidance literature:: With Crabtree's catalyst BAr^F analogue; hydrogen; In 1,2-dichloro-ethane; at 23 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acs.joc.0c00565

Reference yield: 100.0%

: 177949-92-7
(E)-4,4,5,5-tetramethyl-2-(3-methylbut-1-en-1-yl)-1,3,2-dioxaborolane

: 2-(2,4-dimethoxyphenyl)-5-hydroxy-6-iodo-7-methoxy-3-(3-methylbut-2-en-1-yl)-4H-chromen-4-one

: 5916-10-9
(E)-2-(2,4-dimethoxyphenyl)-5-hydroxy-7-methoxy-6-(3-methylbut-1-en-1-yl)-3-(3-methylbut-2-en-1-yl)-4H-chromen-4-one

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; In 1,4-dioxane; water; at 100 ℃; for 9h; Solvent; Inert atmosphere;
DOI:10.3987/COM-15-S(T)42

Reference yield: 42.0%

: 177949-92-7
(E)-4,4,5,5-tetramethyl-2-(3-methylbut-1-en-1-yl)-1,3,2-dioxaborolane

: tert-butyl(2-iodoethoxy)diphenylsilane

: C₂₉H₄₅BO₃Si

Guidance literature:: With potassium fluoride; C₁₈H₁₆N₂O₂; diethoxymethylane; nickel dichloride; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; at 20 ℃; for 40h; enantioselective reaction;
DOI:10.1038/s41557-020-00576-z