3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-triene-4-carboxylic acid phenylamide

Base Information

• Chemical Name: 3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-triene-4-carboxylic acid phenylamide
• CAS No.: 116387-01-0
• Molecular Formula: C₂₁H₂₃NO₅
• Molecular Weight: 369.417

Synonyms:3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-triene-4-carboxylic acid phenylamide

Chemical Property of 3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-triene-4-carboxylic acid phenylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-triene-4-carboxylic acid phenylamide

There total 6 articles about 3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-triene-4-carboxylic acid phenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyl isocyanate (103-71-9) + 3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.02,7]trideca-2(7),3,5-triene (79834-13-2) → 3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.02,7]trideca-2(7),3,5-triene-4-carboxylic acid phenylamide (116387-01-0) + bis(diphenyl)urea (102-07-8)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) ether, hexane, 2.5 h, 2.) ether, hexane, 30 min;

Reference yield:

ethylene-cetal de la bromo-5 pentanone-2 (24400-75-7) → 3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.02,7]trideca-2(7),3,5-triene-4-carboxylic acid phenylamide (116387-01-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) ether, -10 deg C, 3 h, 2.) ether, THF, -10 deg C, 1 h

2: 67.1 percent / conc.sulphuric acid / aq. acetic acid / 26 h

3: 1.) BuLi / 1.) ether, hexane, 2.5 h, 2.) ether, hexane, 30 min

With tetrahydrofuran; n-butyllithium; diethyl ether; sulfuric acid; In acetic acid;

Reference yield:

bromo-5-pentanone-2 (3884-71-7) → 3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.02,7]trideca-2(7),3,5-triene-4-carboxylic acid phenylamide (116387-01-0)

Guidance literature:

Multi-step reaction with 4 steps

1: toluene-p-sulphonic acid hydrate / benzene / 2 h / Heating

2: 1.) ether, -10 deg C, 3 h, 2.) ether, THF, -10 deg C, 1 h

3: 67.1 percent / conc.sulphuric acid / aq. acetic acid / 26 h

4: 1.) BuLi / 1.) ether, hexane, 2.5 h, 2.) ether, hexane, 30 min

With tetrahydrofuran; n-butyllithium; diethyl ether; sulfuric acid; toluene-4-sulfonic acid; In acetic acid; benzene;

upstream raw materials:

phenyl isocyanate

3-Methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-triene

ethylene-cetal de la bromo-5 pentanone-2

bromo-5-pentanone-2

Downstream raw materials:

C₂₄H₂₆O₉

(3,5-Dimethoxy-phenyl)-(4-hydroxymethyl-3-methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-trien-5-yl)-methanol

5-(3,5-Dimethoxy-benzoyl)-3-methoxymethoxy-9-methyl-8,13-dioxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-triene-4-carbaldehyde

C₂₄H₂₆O₈

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