cyclopropyl-{5-[3-(2-dimethylamino-ethoxy)-phenyl]-[2,2';4',3]terpyridin-6'-yl}-amine

Base Information

Chemical Name:cyclopropyl-{5-[3-(2-dimethylamino-ethoxy)-phenyl]-[2,2';4',3]terpyridin-6'-yl}-amine
CAS No.:1171042-36-6
Molecular Formula:C₂₈H₂₉N₅O
Molecular Weight:451.571
Hs Code.:

Synonyms:cyclopropyl-{5-[3-(2-dimethylamino-ethoxy)-phenyl]-[2,2';4',3]terpyridin-6'-yl}-amine

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Chemical Property of cyclopropyl-{5-[3-(2-dimethylamino-ethoxy)-phenyl]-[2,2';4',3]terpyridin-6'-yl}-amine

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Technology Process of cyclopropyl-{5-[3-(2-dimethylamino-ethoxy)-phenyl]-[2,2';4',3]terpyridin-6'-yl}-amine

There total 3 articles about cyclopropyl-{5-[3-(2-dimethylamino-ethoxy)-phenyl]-[2,2';4',3]terpyridin-6'-yl}-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 925940-40-5
dimethyl-{2-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenoxy]-ethyl}-amine

: 1171039-42-1
(5-bromo-[2,2';4',3]terpyridin-6'-yl)-cyclopropyl-amine

: 1171042-36-6
cyclopropyl-{5-[3-(2-dimethylamino-ethoxy)-phenyl]-[2,2';4',3]terpyridin-6'-yl}-amine

Guidance literature:: With sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,2-dimethoxyethane; at 90 ℃; Inert atmosphere of argon; Microwave radiation;

Reference yield:

: 221915-84-0
[2-(3-bromo-phenoxy)ethyl]-dimethyl-arnine

: 1171042-36-6
cyclopropyl-{5-[3-(2-dimethylamino-ethoxy)-phenyl]-[2,2';4',3]terpyridin-6'-yl}-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium acetate / 1,2-dimethoxyethane / Inert atmosphere of N₂

1.2: 100 °C / Microwave radiation

2.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane / 90 °C / Inert atmosphere of argon; Microwave radiation

With potassium acetate; sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,2-dimethoxyethane;

Reference yield:

: 591-20-8
3-Bromophenol

: 1171042-36-6
cyclopropyl-{5-[3-(2-dimethylamino-ethoxy)-phenyl]-[2,2';4',3]terpyridin-6'-yl}-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / NMP (1-methyl-2-pyrrolidone) / 80 °C

2.1: potassium acetate / 1,2-dimethoxyethane / Inert atmosphere of N₂

2.2: 100 °C / Microwave radiation

3.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane / 90 °C / Inert atmosphere of argon; Microwave radiation

With potassium acetate; sodium carbonate; potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,2-dimethoxyethane; NMP (1-methyl-2-pyrrolidone);