-1,3-Cyclohexadien

Base Information

• Chemical Name: -1,3-Cyclohexadien
• CAS No.: 26005-40-3
• Molecular Formula: C₆H₈
• Molecular Weight: 82.1136

Synonyms:-1,3-Cyclohexadien

Chemical Property of -1,3-Cyclohexadien

Chemical Property:

Purity/Quality:

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Technology Process of -1,3-Cyclohexadien

There total 4 articles about -1,3-Cyclohexadien which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

-cis-Cyclohexa-1,2-diyldiacetat (136489-56-0) → -1,3-Cyclohexadien (26005-40-3) + cyclohexene (110-83-8) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1)

Guidance literature:

at 490 ℃; Title compound not separated from byproducts;

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → benzene-d1 (1120-89-4) + benzene-d6 (1076-43-3) + 6-deuterio-cyclohexa-1->5-dienyl + benzene-d5 (13657-09-5) + cyclohexadiene-d6 (55449-47-3) + -1,3-Cyclohexadien (26005-40-3)

Guidance literature:

With D; platinum on activated charcoal; at -153.1 - 26.9 ℃; also (1,4)-dimethylcyclohexane;

DOI:10.1063/1.470934

Reference yield:

→ -1,3-Cyclohexadien (26005-40-3)

Guidance literature:

With trifluoroacetic acid-d₁; Yield given. Multistep reaction; 1.) r. t., 5 min, 2.) MeOH, 2 h;

upstream raw materials:

-cis-Cyclohexa-1,2-diyldiacetat

cyclohexa-1,3-diene

benzene

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