C₅₇H₆₆BrN

Base Information

Chemical Name:C₅₇H₆₆BrN
CAS No.:1373359-05-7
Molecular Formula:C₅₇H₆₆BrN
Molecular Weight:845.062
Hs Code.:

Synonyms:C₅₇H₆₆BrN

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Chemical Property of C₅₇H₆₆BrN

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Technology Process of C₅₇H₆₆BrN

There total 3 articles about C₅₇H₆₆BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1373359-04-6
2,7-dibromo-9,9-bis(4-decylphenyl)-fluorene

: 122-39-4
diphenylamine

: 1373359-05-7
C₅₇H₆₆BrN

Guidance literature:: With palladium diacetate; triphenylphosphine; sodium t-butanolate; In toluene; for 36h; Inert atmosphere; Reflux;
DOI:10.1021/ja302085q

Reference yield:

: methyl 4,4'-dibromo-[1,1'-biphenyl]-2-carboxylate

: 1373359-05-7
C₅₇H₆₆BrN

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: trifluorormethanesulfonic acid / tetrahydrofuran; dichloromethane / 0 - 20 °C

3.1: palladium diacetate; triphenylphosphine; sodium t-butanolate / toluene / 36 h / Inert atmosphere; Reflux

With n-butyllithium; trifluorormethanesulfonic acid; palladium diacetate; triphenylphosphine; sodium t-butanolate; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/ja302085q

Reference yield:

: 106418-67-1
1-bromo-4-n-decyl benzene

: 1373359-05-7
C₅₇H₆₆BrN

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: trifluorormethanesulfonic acid / tetrahydrofuran; dichloromethane / 0 - 20 °C

3.1: palladium diacetate; triphenylphosphine; sodium t-butanolate / toluene / 36 h / Inert atmosphere; Reflux

With n-butyllithium; trifluorormethanesulfonic acid; palladium diacetate; triphenylphosphine; sodium t-butanolate; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/ja302085q