4-dimethylamino-1-(3,5-dichlorophenyl)-2-methylsulfanyl-1,3-diazabuta-1,3-dienium iodide

Base Information

Chemical Name:4-dimethylamino-1-(3,5-dichlorophenyl)-2-methylsulfanyl-1,3-diazabuta-1,3-dienium iodide
CAS No.:1262446-21-8
Molecular Formula:C₁₁H₁₃Cl₂N₃S*HI
Molecular Weight:418.129
Hs Code.:

Synonyms:4-dimethylamino-1-(3,5-dichlorophenyl)-2-methylsulfanyl-1,3-diazabuta-1,3-dienium iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-dimethylamino-1-(3,5-dichlorophenyl)-2-methylsulfanyl-1,3-diazabuta-1,3-dienium iodide

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Technology Process of 4-dimethylamino-1-(3,5-dichlorophenyl)-2-methylsulfanyl-1,3-diazabuta-1,3-dienium iodide

There total 1 articles about 4-dimethylamino-1-(3,5-dichlorophenyl)-2-methylsulfanyl-1,3-diazabuta-1,3-dienium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 477852-00-9
4-dimethylamino-2-(3,5-dichlorophenyl)amino-1,3-thiazabuta-1,3-diene

: 74-88-4
methyl iodide

: 1262446-21-8
4-dimethylamino-1-(3,5-dichlorophenyl)-2-methylsulfanyl-1,3-diazabuta-1,3-dienium iodide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 6h;
DOI:10.1016/j.tet.2010.10.059

Reference yield: 95.0%

: 1262446-21-8
4-dimethylamino-1-(3,5-dichlorophenyl)-2-methylsulfanyl-1,3-diazabuta-1,3-dienium iodide

: 103-80-0
phenylacetyl chloride

: 1262446-35-4
3-(3,5-dichlorophenyl)-2-methylsulfanyl-5-phenylpyrimidin-4(3H)-one

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.tet.2010.10.059

Reference yield: 94.0%

: 1262446-21-8
4-dimethylamino-1-(3,5-dichlorophenyl)-2-methylsulfanyl-1,3-diazabuta-1,3-dienium iodide

: 1262446-24-1
4-dimethylamino-1-(3,5-dichlorophenyl)-2-methylsulfanyl-1,3-diazabuta-1,3-diene

Guidance literature:: With potassium hydrogencarbonate; In diethyl ether; water; at 20 ℃; for 2h; Saturated solution;
DOI:10.1016/j.tet.2010.10.059