N⁴-benzyloxycarbonyl-N⁸-tert-butoxycarbonylspermidine

Base Information Edit

Chemical Name:N⁴-benzyloxycarbonyl-N⁸-tert-butoxycarbonylspermidine
CAS No.:853783-20-7
Molecular Formula:C₂₀H₃₃N₃O₄
Molecular Weight:379.5
Hs Code.:
Mol file:853783-20-7.mol

N<sup>4</sup>-benzyloxycarbonyl-N<sup>8</sup>-tert-butoxycarbonylspermidine

Synonyms:N⁴-benzyloxycarbonyl-N⁸-tert-butoxycarbonylspermidine

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Chemical Property of N⁴-benzyloxycarbonyl-N⁸-tert-butoxycarbonylspermidine Edit

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Technology Process of N⁴-benzyloxycarbonyl-N⁸-tert-butoxycarbonylspermidine

There total 5 articles about N⁴-benzyloxycarbonyl-N⁸-tert-butoxycarbonylspermidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

: 853783-18-3
N¹-benzyloxycarbonyl-N⁴-tert-butoxycarbonyl-N¹-(2-cyanoethyl)-1,4-butanediamine

: 853783-20-7
N⁴-benzyloxycarbonyl-N⁸-tert-butoxycarbonylspermidine

Guidance literature:: With ammonia; hydrogen; In tetrahydrofuran; methanol; at 50 ℃; for 10h; under 22502.3 Torr; Inert atmosphere; Autoclave;
DOI:10.1055/s-0037-1610326

Reference yield:

: 68076-40-4
N¹-tert-butoxycarbonyl-N⁴-(2-cyanoethyl)-1,4-butanediamine

: 853783-20-7
N⁴-benzyloxycarbonyl-N⁸-tert-butoxycarbonylspermidine

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / triethylamine / tetrahydrofuran

2: 61 percent / LiAlH₄ / diethyl ether / 0 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1081/SCC-200054211

Reference yield:

: 68076-36-8
1-amino-4-[(tert-butyloxycarbonyl)amino]butane

: 853783-20-7
N⁴-benzyloxycarbonyl-N⁸-tert-butoxycarbonylspermidine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 20 °C

2: triethylamine / tetrahydrofuran / 20 °C

3: ammonia; hydrogen / methanol / 50 °C / 37503.8 - 75007.5 Torr / Autoclave

With ammonia; hydrogen; triethylamine; In tetrahydrofuran; methanol;