1,8-Diphenyl-11,11-bis-trimethylsilanyl-11-sila-tricyclo[6.2.1.0^2,7]undeca-2⁽⁷⁾,3,5,9-tetraene

Base Information

• Chemical Name: 1,8-Diphenyl-11,11-bis-trimethylsilanyl-11-sila-tricyclo[6.2.1.0^2,7]undeca-2⁽⁷⁾,3,5,9-tetraene
• CAS No.: 83363-82-0
• Molecular Formula: C₂₈H₃₄Si₃
• Molecular Weight: 454.834

Synonyms:1,8-Diphenyl-11,11-bis-trimethylsilanyl-11-sila-tricyclo[6.2.1.0^2,7]undeca-2⁽⁷⁾,3,5,9-tetraene

Chemical Property of 1,8-Diphenyl-11,11-bis-trimethylsilanyl-11-sila-tricyclo[6.2.1.0^2,7]undeca-2⁽⁷⁾,3,5,9-tetraene

Chemical Property:

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Technology Process of 1,8-Diphenyl-11,11-bis-trimethylsilanyl-11-sila-tricyclo[6.2.1.0^2,7]undeca-2⁽⁷⁾,3,5,9-tetraene

There total 1 articles about 1,8-Diphenyl-11,11-bis-trimethylsilanyl-11-sila-tricyclo[6.2.1.0^2,7]undeca-2⁽⁷⁾,3,5,9-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

2,5-Diphenyl-1,1-bis-trimethylsilanyl-1H-silole (83363-85-3) + 1H-1,2,3-benzotriazol-1-amine (1614-12-6) → 1,8-Diphenyl-11,11-bis-trimethylsilanyl-11-sila-tricyclo[6.2.1.02,7]undeca-2(7),3,5,9-tetraene (83363-82-0)

Guidance literature:

With lead(IV) acetate; In dichloromethane; at 0 ℃; for 0.166667h;

DOI:10.1021/ja00386a072

Reference yield: 50.0%

1,8-Diphenyl-11,11-bis-trimethylsilanyl-11-sila-tricyclo[6.2.1.02,7]undeca-2(7),3,5,9-tetraene (83363-82-0) + 2,3-dimethyl-buta-1,3-diene (513-81-5) → 1,4-diphenylnaphthalene (796-30-5) + 3,4-dimethyl-1,1-bis-trimethylsilanyl-2,5-dihydro-1H-silole (51650-56-7)

Guidance literature:

at 220 ℃; for 2h;

DOI:10.1021/ja00386a072

upstream raw materials:

2,5-Diphenyl-1,1-bis-trimethylsilanyl-1H-silole

1H-1,2,3-benzotriazol-1-amine

Downstream raw materials:

1,4-diphenylnaphthalene

3,4-dimethyl-1,1-bis-trimethylsilanyl-2,5-dihydro-1H-silole

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