tert-butyl 5-(3-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropylamino)phenoxy)pentylcarbamate

Base Information

Chemical Name:tert-butyl 5-(3-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropylamino)phenoxy)pentylcarbamate
CAS No.:1262543-65-6
Molecular Formula:C₃₁H₃₇Br₂N₃O₄
Molecular Weight:675.46
Hs Code.:

Synonyms:tert-butyl 5-(3-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropylamino)phenoxy)pentylcarbamate

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Chemical Property of tert-butyl 5-(3-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropylamino)phenoxy)pentylcarbamate

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Technology Process of tert-butyl 5-(3-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropylamino)phenoxy)pentylcarbamate

There total 5 articles about tert-butyl 5-(3-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropylamino)phenoxy)pentylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1262543-64-5
3-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropylamino)phenol

: 142342-55-0
diethyl {5-[(tert-butoxycarbonyl)amino]pentyl }-propanedioate

: 1262543-65-6
tert-butyl 5-(3-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropylamino)phenoxy)pentylcarbamate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃;
DOI:10.1021/ja108211m

Reference yield:

: 313268-18-7
1-(3,6-dibromo-9H-carbazol-9-yl)-3-((3-methoxyphenyl)amino)propan-2-ol

: 1262543-65-6
tert-butyl 5-(3-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropylamino)phenoxy)pentylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: boron tribromide / dichloromethane / 0.08 h / Cooling with ice

2: potassium carbonate / N,N-dimethyl-formamide / 90 °C

With boron tribromide; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja108211m

Reference yield:

: 6825-20-3
3,6-dibromo-9H-carbazole

: 1262543-65-6
tert-butyl 5-(3-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-hydroxypropylamino)phenoxy)pentylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 20 °C

2.1: bismuth(III) chloride / cyclohexane / Reflux

3.1: boron tribromide / dichloromethane / 0.08 h / Cooling with ice

4.1: potassium carbonate / N,N-dimethyl-formamide / 90 °C

With bismuth(III) chloride; boron tribromide; potassium carbonate; potassium hydroxide; In dichloromethane; cyclohexane; N,N-dimethyl-formamide;
DOI:10.1021/ja108211m