methyl-3-<3-<4-(3-t-butyldimethylsilylether-1-propynyl)phenoxy>-4-methoxyphenyl> propionate

Base Information

Chemical Name:methyl-3-<3-<4-(3-t-butyldimethylsilylether-1-propynyl)phenoxy>-4-methoxyphenyl> propionate
CAS No.:168135-08-8
Molecular Formula:C₂₆H₃₄O₅Si
Molecular Weight:454.638
Hs Code.:

Synonyms:methyl-3-<3-<4-(3-t-butyldimethylsilylether-1-propynyl)phenoxy>-4-methoxyphenyl> propionate

Suppliers and Price of methyl-3-<3-<4-(3-t-butyldimethylsilylether-1-propynyl)phenoxy>-4-methoxyphenyl> propionate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl-3-<3-<4-(3-t-butyldimethylsilylether-1-propynyl)phenoxy>-4-methoxyphenyl> propionate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl-3-<3-<4-(3-t-butyldimethylsilylether-1-propynyl)phenoxy>-4-methoxyphenyl> propionate

There total 8 articles about methyl-3-<3-<4-(3-t-butyldimethylsilylether-1-propynyl)phenoxy>-4-methoxyphenyl> propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 129150-61-4
3-(3-hydroxy-4-methoxyphenyl)-propionic acid methyl ester

: 168135-07-7
3-(4-bromophenyl)-2-propyn-1-t-butyldimethylsilyl ether

: 168135-08-8
methyl-3-<3-<4-(3-t-butyldimethylsilylether-1-propynyl)phenoxy>-4-methoxyphenyl> propionate

Guidance literature:: With pyridine; potassium carbonate; copper(II) oxide; at 120 ℃; for 12h;
DOI:10.1080/00397919508015470

Reference yield:

: 621-59-0
isovanillin

: 168135-08-8
methyl-3-<3-<4-(3-t-butyldimethylsilylether-1-propynyl)phenoxy>-4-methoxyphenyl> propionate

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / pyridine, piperidine / 3 h / Heating

2: 97 percent / p-TsOH / 24 h / Heating

3: 100 percent / H₂ / 10percent Pd/C / aq. ethanol / Ambient temperature

4: 74 percent / CuO, K₂CO₃, pyridine / 12 h / 120 °C

With piperidine; pyridine; hydrogen; potassium carbonate; toluene-4-sulfonic acid; copper(II) oxide; palladium on activated charcoal; In ethanol;
DOI:10.1080/00397919508015470

Reference yield:

: 97966-29-5
methyl (E)-3-(3-hydroxy-4-methoxyphenyl)-2-propenoate

: 168135-08-8
methyl-3-<3-<4-(3-t-butyldimethylsilylether-1-propynyl)phenoxy>-4-methoxyphenyl> propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / 10percent Pd/C / aq. ethanol / Ambient temperature

2: 74 percent / CuO, K₂CO₃, pyridine / 12 h / 120 °C

With pyridine; hydrogen; potassium carbonate; copper(II) oxide; palladium on activated charcoal; In ethanol;
DOI:10.1080/00397919508015470