2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside
CAS No.:136090-72-7
Molecular Formula:C₅₄H₅₈O₁₁
Molecular Weight:883.048
Hs Code.:

Synonyms:2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside

Suppliers and Price of 2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside

There total 11 articles about 2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 149113-51-9
2,3,2',3'-tetra-O-benzyl-4,6;4',6'-di-O-benzylidene-α,α-D-trehalose

: 136090-72-7
2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With aluminium trichloride; trimethylamine-borane; In tetrahydrofuran;
DOI:10.1021/ol026095m

Reference yield: 55.0%

: 149113-51-9
2,3,2',3'-tetra-O-benzyl-4,6;4',6'-di-O-benzylidene-α,α-D-trehalose

: 1456898-33-1
2,3,4,2',3'-penta-O-benzyl-4',6'-O-benzylidene-α,α-D-trehalose

: 132183-33-6
2,3,6-tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzylidene-α-D-glucopyranoside

: 136090-72-7
2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at 0 - 20 ℃; for 1.5h; regioselective reaction; Inert atmosphere;
DOI:10.1080/14756366.2020.1837125

Reference yield:

: 99-20-7
TREHALOSE

: 100-39-0
benzyl bromide

: 136090-72-7
2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 103128-34-3
2,3,4,6,2',3',6'-hepta-O-benzyl-α,α-D-trehalose

Guidance literature:: TREHALOSE; With benzaldehyde dimethyl acetal; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 100 ℃; for 5.66667h; under 160 Torr;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; paraffin oil; at 20 ℃; for 45h; Cooling with ice;

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h; Solvent;