2,3,4,6,2',3',6'-hepta-O-benzyl-α,α-D-trehalose

Base Information

Chemical Name:2,3,4,6,2',3',6'-hepta-O-benzyl-α,α-D-trehalose
CAS No.:103128-34-3
Molecular Formula:C₆₁H₆₄O₁₁
Molecular Weight:973.173
Hs Code.:

Synonyms:2,3,4,6,2',3',6'-hepta-O-benzyl-α,α-D-trehalose

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Chemical Property of 2,3,4,6,2',3',6'-hepta-O-benzyl-α,α-D-trehalose

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Technology Process of 2,3,4,6,2',3',6'-hepta-O-benzyl-α,α-D-trehalose

There total 6 articles about 2,3,4,6,2',3',6'-hepta-O-benzyl-α,α-D-trehalose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.7%

: 116594-37-7
2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-benzylidene-α,α-trehalose

: 103128-34-3
2,3,4,6,2',3',6'-hepta-O-benzyl-α,α-D-trehalose

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; dichloromethane; for 2h; Heating;
DOI:10.1016/0008-6215(88)84146-6

Reference yield: 49.0%

: 116594-37-7
4,6-O-benzylidene-2,3,2’,3’4’,6’-hexa-O-benzyl-α,α’-trehalose

: 103128-34-3
2,3,4,6,2',3',6'-hepta-O-benzyl-α,α-D-trehalose

: 103128-35-4
2,3,4,2’,3’,4’,6’-hepta-O-benzyl-α,α’-trehalose

Guidance literature:: With aluminum (III) chloride; trimethylamine-borane; In tetrahydrofuran; at 0 ℃; for 16h; Inert atmosphere; Molecular sieve;
DOI:10.1080/14756366.2020.1837125

Reference yield:

: 99-20-7
TREHALOSE

: 100-39-0
benzyl bromide

: 136090-72-7
2,3,6-Tri-O-benzyl-α-D-glucopyranosyl 2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 103128-34-3
2,3,4,6,2',3',6'-hepta-O-benzyl-α,α-D-trehalose

Guidance literature:: TREHALOSE; With benzaldehyde dimethyl acetal; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 100 ℃; for 5.66667h; under 160 Torr;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; paraffin oil; at 20 ℃; for 45h; Cooling with ice;

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h; Solvent;